4-(苄氧基)-5-甲氧基-2-硝基苯甲醛合成路线 （共 24 条）
反应条件
nitric acid T=0°C; 1 h;
参考文献
Tsai, Shiou-Chuan; Klinman, Judith P.
Bioorganic Chemistry, 2003 , vol. 31, # 2 p. 172 - 190
反应条件
potassium carbonate in N,N-dimethyl-formamide T=100°C; 2 h;
参考文献
Kobayashi, Shigeru; Okimoto, Kazuto; Imakura, Yasuhiro
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 5 p. 1567 - 1573
反应条件
benzyltriphenylphosphonium peroxodisulfate in acetonitrile Oxidation; decarboxylation; 1 h; Heating;
参考文献
Mohammadpoor-Baltork, Iraj; Hajipour, Abdol Reza; Mohammadi, Hasan
Bulletin of the Chemical Society of Japan, 1998 , vol. 71, # 7 p. 1649 - 1653
反应条件
1: 95 percent / K2CO3 / acetone / 4 h / Heating 2: 78 percent / HNO3; H2SO4; AcOH / 1 h / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 15, # 14 p. 3369 - 3373
反应条件
1: 95 percent / K2CO3 / acetone / 4 h / Heating 2: 78 percent / HNO3; H2SO4; AcOH / 1 h / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 15, # 14 p. 3369 - 3373
反应条件
1: 72 percent / methanol; dimethylsulfoxide; dimethylformamide / 2 h / 150 °C 2: 90 percent / K2CO3 / dimethylformamide / 2 h / 100 °C View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 30, # 5 p. 1567 - 1573
反应条件
1: 7 percent / phenylmethanol; dimethylsulfoxide / 0.02 h / 150 °C 2: 12 mg / 2 percent NaOH / 1 h / 85 °C View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 30, # 5 p. 1567 - 1573
反应条件
sodium hydroxide T=85°C; 1 h;
参考文献
Kobayashi, Shigeru; Okimoto, Kazuto; Imakura, Yasuhiro
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 5 p. 1567 - 1573
反应条件
1: KOH / ethanol / Heating 2: NO2/HNO3 / acetic acid View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 1417 - 1423
反应条件
ammonium acetate in acetic acid Heating;
参考文献
Kissei Pharmaceutical Co., Ltd.
Patent: EP2133332 A1, 2009 ;
Location in patent: Page/Page column 28-29 ;
EP 2133332 A1
