4-苄氧基-3-甲氧基苯甲醛合成路线 （共 139 条）
反应条件
1: 69 percent / sodium acetate; bromine / acetic acid / 11 h / 40 °C 2: NaBH4 / tetrahydrofuran / 4 h / 0 °C 3: CBr4; triphenylphosphine / methanol / 20 °C View Scheme
参考文献
Fukuyama, Yoshiyasu; Yaso, Hideyuki; Mori, Takashi; Takahashi, Hironobu; Minami, Hiroyuki; Kodama, Mitsuaki
Heterocycles, 2001 , vol. 54, # 1 p. 259 - 274
反应条件
1: zinc; ammonium chloride; (R)-TRIP-BINOL / toluene; di-isopropyl ether / 16 h / 4 °C / |Inert atmosphere 2: [RhCl(η2:η2-cycloocta-1,5-diene)]2; triethylamine / 1,4-dioxane; water / 2 h / 90 °C / |Inert atmosphere 3: palladium on activated carbon; hydrogen / ethyl acetate / 16 h / 760.05 Torr / |Inert atmosphere View Scheme
参考文献
Fuchs, Michael; Schober, Markus; Orthaber, Andreas; Faber, Kurt
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 13 p. 2499 - 2505
反应条件
amberlyst-15 T=110°C; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 71, # 7 p. 2892 - 2895
反应条件
iron(III) chloride on silica in neat (no solvent) T=30°C; 1 h;
参考文献
Jempty, Thomas C.; Gogins, Kitty A. Z.; Mazur, Yehuda; Miller, Larry L.
Journal of Organic Chemistry, 1981 , vol. 46, # 22 p. 4545 - 4551
反应条件
amberlyst-15 T=110°C; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 71, # 7 p. 2892 - 2895
参考文献
Boehringer and Soehne
Patent: DE65937 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 3, p. 897
参考文献
Riedel-de Haen
Patent: DE549432 , 1926 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 575
反应条件
1: NH4OAc / acetic acid / Heating 2: NO2/HNO3 / acetic acid View Scheme
参考文献
Julia,M. et al.
Bulletin de la Societe Chimique de France, 1965 , p. 1417 - 1423
反应条件
(i) NO2/HNO3, (ii) H2SO4; Multistep reaction;
参考文献
Rogers, C. Bradford; Blum, Charles A.; Murphy, Bryan P.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 941 - 943
反应条件
1: hydrazine hydrate / bis-(2-hydroxy-ethyl) ether / 0.17 h / Irradiation 2: KOH / bis-(2-hydroxy-ethyl) ether / 0.28 h / Irradiation View Scheme
参考文献
Chattopadhyay, Sarmishtha; Banerjee, Sajal Kumar; Mitra, Alok Kumar
Journal of the Indian Chemical Society, 2002 , vol. 79, # 11 p. 906 - 907
