4-苄氧基-3-甲氧基苯甲醛合成路线 （共 139 条）
反应条件
sodium chlorite; sodium dihydrogenphosphate; dihydrogen peroxide in water; acetonitrile T=20°C; 1.5 h;
参考文献
Correa, Arkaitz; Tellitu, Imanol; Dominguez, Esther; Moreno, Isabel; SanMartin, Raul
Journal of Organic Chemistry, 2005 , vol. 70, # 6 p. 2256 - 2264
反应条件
potassium hydroxide in methanol T=90°C; Cannizzaro reaction; 3 h;
参考文献
European Journal of Organic Chemistry, , # 32 p. 5376 - 5385
反应条件
sodium in diethyl ether 5.5 h; Heating;
参考文献
Ahvonen, Toivo; Brunow, Goesta; Kristersson, Per; Lundquist, Knut
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 9 p. 845 - 850
反应条件
1: With sodium chlorite; sodium dihydrogenphosphate; dihydrogen peroxide in water; acetonitrile T=10 - 20°C; 1.5 h; 2: With sodium thiosulfate in water; acetonitrile 0.0833333 h;
参考文献
Zhao, Chao; Liu, Zai-Qun
Biochimie, 2013 , vol. 95, # 4 p. 842 - 849
反应条件
1: lithium diisopropyl amide / tetrahydrofuran / -78 °C 2: sodium tetrahydroborate / tetrahydrofuran; water 3: palladium on activated charcoal; hydrogen / methanol 4: 4-acetylamino 2,2,6,6-tetramethylpiperidin-N-oxyl; oxygen; nitric acid; hydrogenchloride / water; acetonitrile / 24 h / 45 °C / |High pressure; |Sealed tube View Scheme
参考文献
Rahimi, Alireza; Azarpira, Ali; Kim, Hoon; Ralph, John; Stahl, Shannon S.
Journal of the American Chemical Society, 2013 , vol. 135, # 17 p. 6415 - 6418
反应条件
1: acetic acid; ammonium acetate / 100 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / |Reflux 3: ethanol / 14 h / |Reflux 4: pyridine / dichloromethane / 1.5 h / 0 - 20 °C 5: trichlorophosphate / acetonitrile / 1 h / |Reflux; |Inert atmosphere 6: [[(η6-p-cymene)((1S,2S)-N-p-toluenesulfonyl-1,2-diphenylethylenediamine)]Ru]; formic acid; triethylamine / N,N-dimethyl-formamide / 20 °C 7: water; sodium hydroxide / ethanol / 3 h / 20 °C 8: thionyl chloride / dichloromethane / 1.5 h / 0 - 20 °C 9: sodium hydrogencarbonate / dichloromethane / 1.5 h / 20 °C 10: hydrogenchloride / water; ethanol / 2 h / |Reflux View Scheme
参考文献
Sun, Haifeng; Zhu, Liyuan; Yang, Huicui; Qian, Wangke; Guo, Lin; Zhou, Shengbin; Gao, Bo; Li, Zeng; Zhou, Yu; Jiang, Hualiang; Chen, Kaixian; Zhen, Xuechu; Liu, Hong
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 4 p. 856 - 868
反应条件
1: NaBH4 / methanol / 20 °C 2: SOCl2 / dioxane / 20 °C 3: acetonitrile / 20 °C View Scheme
参考文献
Waddell, Thomas G.; Rapoport, Henry
Phytochemistry (Elsevier), 1985 , vol. 24, # 3 p. 469 - 472
反应条件
1: pyridine; piperidine / 3 h / 80 - 95 °C 2: sulfuric acid / 2 h / Heating 3: N,N-dimethylaniline; AlCl3 / CH2Cl2 / 2 h / 0 - 5 °C View Scheme
参考文献
Venkateswarlu, Somepalli; Ramachandra, Mareullapudi S.; Krishnaraju, Alluri V.; Trimurtulu, Golakoti; Subbaraju, Gottumukkala V.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 1 p. 252 - 257
反应条件
ammonium acetate in ethanol 5 h; Reflux;
参考文献
Von Nussbaum, Franz; Rueth, Matthias; Spiteller, Peter; Huebscher-Weissert, Tina; Loebermann, Florian; Polborn, Kurt; Steglich, Wolfgang
European Journal of Organic Chemistry, 2012 , # 2 p. 380 - 390
反应条件
1: diethyl ether; tetrahydrofuran / 1 h / 20 °C 2: NaO-tBu; cyclohexanone / toluene / 0.5 h / Heating 3: ammonium formate / 10percent Pd/C / methanol / 0.5 h / Heating 4: 71 percent / 70percent HNO3; AcOH / 0.5 h / 20 °C 5: AlCl3; pyridine / ethyl acetate / 2 h / Heating View Scheme
参考文献
Learmonth, David A.; Vieira-Coelho, Maria A.; Benes, Jan; Alves, Paula C.; Borges, Nuno; Freitas, Ana P.; Soares-da-Silva, Patricio
Journal of Medicinal Chemistry, 2002 , vol. 45, # 3 p. 685 - 695
