烯丙基 2,3,4-三-O-苄基-6-脱氧-beta-L-吡喃半乳糖苷合成路线 （共 3 条）
反应条件
sodium hydride in N,N-dimethyl-formamide T=20°C; 2.5 h;
参考文献
E Silva, Maria Joselice; Srivastava, Rajendra M.; Doboszewski, Bogdan; Cottier, Louis; Sinou, Denis
Heterocyclic Communications, 2010 , vol. 16, # 2-3 p. 105 - 111
反应条件
1: H(+) / 1 h / Heating 2: NaH / dimethylformamide / 20 °C View Scheme
参考文献
E Silva, Maria Joselice; Srivastava, Rajendra M.; Doboszewski, Bogdan; Cottier, Louis; Sinou, Denis
Heterocyclic Communications, 2010 , vol. 16, # 2-3 p. 105 - 111
反应条件
1: With [bis(methyldiphenylphosphine)(1,5-cyclooctadiene)]iridium (1) hexafluorophosphate; hydrogen in tetrahydrofuran T=25°C; 16 h; 2: With iodine; sodium hydrogencarbonate in tetrahydrofuran; water T=25°C; 16 h; optical yield given as percent de;
参考文献
Wiebe, Christine; Schlemmer, Claudine; Weck, Stefan; Opatz, Till
Chemical Communications, 2011 , vol. 47, # 32 p. 9212 - 9214
