反应条件
1: 2-Bromo-3-iodothiophene With ethyl magnesium chloride in tetrahydrofuran
T=0°C; Inert atmosphere;
2: N,N-dimethyl-formamide in tetrahydrofuran
T=0°C; Inert atmosphere;
3: With water; ammonium chloride in tetrahydrofuran
Inert atmosphere;
参考文献
Sonoda, Motohiro; Kinoshita, Shoko; Luu, Thanh; Fukuda, Hiroshi; Miki, Koji; Umeda, Rui; Tobe, Yoshito
Synthetic Communications, 2009 , vol. 39, # 18 p. 3315 - 3323
