苯并[b]萘并[2,3-d]呋喃合成路线 （共 32 条）
反应条件
[Ni0(1,5-cyclooctadiene)2]; caesium carbonate; dcype in anhydrous xylene T=160°C; 72 h;
参考文献
Tetrahedron, , vol. 69, # 27-28 p. 5780 - 5790
反应条件
bis(triphenylphosphine)palladium(II)-chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride in N,N-dimethyl-formamide T=145°C;
参考文献
Tetrahedron, , vol. 58, # 29 p. 5927 - 5931
反应条件
2Ag(1+)*CH2O3(2-); Pd(TFA)2 in 1,4-dioxane; dimethyl sulfoxide T=150°C; 14 h; Inert atmosphere; regioselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 131, p. 4194 - 4195
反应条件
3-NO2-pyridine; tertiary butyl peroxybenzenoate; palladium diacetate in 1,3-dimethyl-imidazolidin-2-one; hexafluorobenzene T=90°C; 4 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 13, # 20 p. 5504 - 5507
反应条件
zinc dibromide in 1,2-dichloro-ethane T=20°C; Inert atmosphereReflux;
参考文献
European Journal of Organic Chemistry, , # 5 p. 922 - 935
反应条件
potassium carbonate; copper(II) oxide in pyridine Ullman reaction; 4 h; Heating;
参考文献
Tetrahedron, , vol. 61, # 5 p. 1353 - 1362
反应条件
palladium diacetate; caesium carbonate; CsO2CCMe3; dcype in anhydrous xylene T=140°C; 17 h; GloveboxSealed tube; Overall yield = 84 percent; Overall yield = 60.1 mg;
参考文献
Organic Letters, , vol. 14, # 18 p. 4838 - 4841,4
Organic Letters, , vol. 14, # 18 p. 4838 - 4841
反应条件
1.1: 98 percent / hydrogen / Pd/C / ethyl acetate / 1.25 h / 20 °C / 760 Torr 2.1: NaBH4 / methanol / 1.5 h / 0 - 20 °C 3.1: 0.638 g / sulfuric acid / 0.5 h / Heating 4.1: O3 / CH2Cl2 / 0.03 h / -78 °C 4.2: 73 percent / dimethyl sulfide / CH2Cl2 / 20 h / -78 - 20 °C 5.1: 100 percent / NaOH / H2O / 1 h / 20 °C 6.1: 73 percent / CuO; potassium carbonate / pyridine / 4 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 61, # 5 p. 1353 - 1362
反应条件
1.1: 98 percent / sodium methoxide / methanol / 15 h / 20 °C 2.1: 98 percent / hydrogen / Pd/C / ethyl acetate / 1.25 h / 20 °C / 760 Torr 3.1: NaBH4 / methanol / 1.5 h / 0 - 20 °C 4.1: 0.638 g / sulfuric acid / 0.5 h / Heating 5.1: O3 / CH2Cl2 / 0.03 h / -78 °C 5.2: 73 percent / dimethyl sulfide / CH2Cl2 / 20 h / -78 - 20 °C 6.1: 100 percent / NaOH / H2O / 1 h / 20 °C 7.1: 73 percent / CuO; potassium carbonate / pyridine / 4 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 61, # 5 p. 1353 - 1362
反应条件
T=650°C; P=0.001 Torr; 1 h; Flash vacuum pyrolysis;
参考文献
Organic and Biomolecular Chemistry, , vol. 8, # 13 p. 2961 - 2967
