苯并[b]萘并[2,3-d]噻吩合成路线 (共 19 条)
反应条件
nickel in ethanol T=78.3°C; 1 h; Rate constant;
参考文献
Nagai, Masatoshi; Urimoto, Hideo; Uetake, Kazuya; Sakikawa, Noriyuki; Gonzalez, Richard D.
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 2 p. 557 - 562
反应条件
trifluorormethanesulfonic acid in dichloromethane
T=0 - 20°C; 2 h; Inert atmosphere;
参考文献
Rafiq, Settu Muhamad; Sivasakthikumaran, Ramakrishnan; Mohanakrishnan, Arasambattu K.
Organic Letters, 2014 , vol. 16, # 10 p. 2720 - 2723
反应条件
zinc dibromide in 1,2-dichloro-ethane
T=20°C; Inert atmosphereReflux;
参考文献
Sureshbabu, Radhakrishnan; Saravanan, Velu; Dhayalan, Vasudevan; Mohanakrishnan, Arasambattu K.
European Journal of Organic Chemistry, 2011 , # 5 p. 922 - 935
反应条件
1: With zinc dibromide in 1,2-dichloro-ethane
T=20°C; Inert atmosphere;
2: in 1,2-dichloro-ethane
T=80°C; Inert atmosphere;
参考文献
Dhayalan, Vasudevan; Clement, J. Arul; Jagan, Radhakrishnan; Mohanakrishnan, Arasambattu K.
European Journal of Organic Chemistry, 2009 , # 4 p. 531 - 546
反应条件
1: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / tetrachloromethane / Reflux
2: zinc dibromide / 1,2-dichloro-ethane / 20 °C / Inert atmosphere; Reflux
View Scheme
参考文献
Sureshbabu, Radhakrishnan; Saravanan, Velu; Dhayalan, Vasudevan; Mohanakrishnan, Arasambattu K.
European Journal of Organic Chemistry, 2011 , # 5 p. 922 - 935
反应条件
1: indium tribromide / 20 °C / Inert atmosphere
2: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / tetrachloromethane / Reflux
3: zinc dibromide / 1,2-dichloro-ethane / 20 °C / Inert atmosphere; Reflux
View Scheme
参考文献
Sureshbabu, Radhakrishnan; Saravanan, Velu; Dhayalan, Vasudevan; Mohanakrishnan, Arasambattu K.
European Journal of Organic Chemistry, 2011 , # 5 p. 922 - 935
参考文献
Komppa
Norske Vid. Selsk. Forh., 1936 , vol. 9, p. 157,159
反应条件
diphosphorus pentasulfide
参考文献
Kruber; Rappen
Chemische Berichte, 1940 , vol. 73, p. 1184
反应条件
1: KOH / 280 - 320 °C
2: phosphorus (V)-sulfide
View Scheme
参考文献
Kruber; Rappen
Chemische Berichte, 1940 , vol. 73, p. 1184
反应条件
1: ethanol / Erhitzen des Reaktionsprodukts mit Phosphor(V)-oxid in Xylol
2: selenium / 350 °C
View Scheme
参考文献
Wilputte; Martin
Bulletin des Societes Chimiques Belges, 1956 , vol. 65, p. 874,891