1-(4-甲基苯基)-2-苯基乙烷-1,2-二酮合成路线 （共 60 条）
反应条件
1: 80 percent / 15percent aq. H2SO4 / tetrahydrofuran / Ambient temperature 2: 88 percent / NH4NO3, glacial AcOH / 16 h / Heating View Scheme
参考文献
Synthesis, , # 10 p. 799 - 801
反应条件
1: (i) THF, (ii) /BRN= 471389/, CuBr 2: HCl / diethyl ether View Scheme
参考文献
Tetrahedron, , vol. 34, p. 1585 - 1592
反应条件
1: MCPBA 2: (i) THF, (ii) /BRN= 471389/, CuBr 3: HCl / diethyl ether View Scheme
参考文献
Tetrahedron, , vol. 34, p. 1585 - 1592
反应条件
carbon monoxide; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran byproducts: (p-Tol)2CO; High Pressure; 0.5 mmol PhCOCl, 1 mmol (p-Tol)2Zn, 2 mmol MgClBr, 0.05 mmol Pd complex,20 ml THF, CO 30 atm, stirred at 25°C for 16 h; GC-MS, GC;
参考文献
Journal of Organometallic Chemistry, , vol. 356, p. 125 - 132
反应条件
1: sodium hydride / mineral oil; tetrahydrofuran / 16.33 h / |Inert atmosphere; |Reflux 2: tert.-butylnitrite; anhydrous iron chloride / 12 h / 30 °C View Scheme
参考文献
RSC Advances, , vol. 4, # 13 p. 6417 - 6423
反应条件
anhydrous lithium nitrate in water; acetonitrile Electrochemical reaction;
参考文献
Australian Journal of Chemistry, , vol. 60, # 6 p. 420 - 428
反应条件
1: AlCl3 / 0 to 25 deg C, 1-2 h 2: bromine / CHCl3 3: 77 percent / DMSO / 4 h / 100 - 120 °C View Scheme
参考文献
Archiv der Pharmazie, , vol. 326, # 1 p. 45 - 50
反应条件
1: SOCl2 / 3 h 2: AlCl3 / 0.75 h / 20 °C 3: 77 percent / SeO2 / dimethylsulfoxide / 0.01 h / microwave irradiation View Scheme
参考文献
Chemistry of Heterocyclic Compounds, , vol. 42, # 7 p. 901 - 906
反应条件
1: 85 percent / bis(trifluoroacetoxy)iodobenzene, water / CHCl3 / 3 h / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 23, # 10 p. 1967 - 1969
Zhurnal Organicheskoi Khimii, , vol. 23, # 10 p. 2225 - 2227
反应条件
1: 85 percent / bis(trifluoroacetoxy)iodobenzene, water / CHCl3 / 3 h / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 23, # 10 p. 1967 - 1969
Zhurnal Organicheskoi Khimii, , vol. 23, # 10 p. 2225 - 2227
