1-(4-甲基苯基)-2-苯基乙烷-1,2-二酮合成路线 (共 60 条)
反应条件
carbon monoxide; Zn(C6H4-4-Me)2; BrClMg; Pd Complex; palladium in tetrahydrofuran P=22800 Torr; 16 h; Ambient temperaturevar. Pd complexes, ethylmetals; Product distribution;
参考文献
Journal of Organometallic Chemistry, , vol. 356, p. 125 - 132
反应条件
sodium hydroxide; selenium(IV) oxide 1.) DMF, 78-80 deg C; 2.) THF, r.t.; Yield given. Multistep reaction;
参考文献
Synlett, , vol. 1997, # 6 p. 671 - 672
反应条件
carbon monoxide in tetrahydrofuran byproducts: (p-Tol)2CO; High Pressure; 0.05 mmol Pd compound, 0.1 mmol (p-Tol)2Zn, 2.5 ml THF, CO 30 atm (at -50°), stirred at 25°C for 2 h in presence of 0.2 mmol MgClBr; GC-MS, GC;
参考文献
Journal of Organometallic Chemistry, , vol. 356, p. 125 - 132
反应条件
samarium diiodide T=20°C; 0.166667 h;
参考文献
Liu, Yongjun; Xu, Xiaoliang; Zhang, Yongmin
Tetrahedron, 2004 , vol. 60, # 22 p. 4867 - 4873
反应条件
9,10-anthracenedicarbonitrile in benzene-d6 Irradiationother amino ketone; Mechanism;
参考文献
Journal of the American Chemical Society, , vol. 114, # 23 p. 8810 - 8812
反应条件
hydrogenchloride; sodium hexamethyldisilazane 1) THF, 6 h, -30 deg C, 2) ether, r. t.; Yield given. Multistep reaction;
参考文献
Angewandte Chemie, , vol. 95, # 8 p. 635
反应条件
potassium hydroxide in methanol; water T=25°C; Kinetics;
参考文献
Journal of Organic Chemistry, , vol. 78, # 14 p. 7194 - 7198
反应条件
lithium diisopropyl amide in tetrahydrofuran T=-30°C; 6 h; crossing experiments;
参考文献
Angewandte Chemie, , vol. 95, # 8 p. 635
反应条件
in dichloromethane T=-20°C; Product distributionMechanism;
参考文献
Chemische Berichte, , vol. 119, # 7 p. 2220 - 2232
反应条件
in dichloromethane; pentane T=-5°C; 1.5 h; Product distributionMechanism;
参考文献
Chemische Berichte, , vol. 119, # 7 p. 2220 - 2232