3,4,5-三甲氧基苯胺合成路线 （共 68 条）
反应条件
hydrazine hydrate; palladium 10 on activated carbon in ethanol 1 h; Reflux;
参考文献
CENTAURUS BIOPHARMA CO., LTD.; XIAO, Dengming; CHENG, Liang; LIU, Xijie; HU, Yuandong; XU, Xinhe; LIU, Zhihua; ZHANG, Lipeng; WU, Wei; WANG, Shulong; SHEN, Yu; LI, Gen; WANG, Yin; ZHAO, Sheng; LI, Chonglong; TANG, Jia; YU, Honghao
Patent: WO2012/92880 A1, 2012 ;
Location in patent: Page/Page column 60 ;
WO 2012/092880 A1
反应条件
4,4'-diphenylsulfide; hydrogen; palladium on activated charcoal in methanol T=20°C; P=760 Torr; 24 h;
参考文献
Mori, Akinori; Mizusaki, Tomoteru; Miyakawa, Yumi; Ohashi, Eri; Haga, Tomoko; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2006 , vol. 62, # 51 p. 11925 - 11932
反应条件
NaClO; sodium hydroxide in water T=20 - 100°C;
参考文献
Qin, Qi-Xue; Yang, Jian; Chen, Duo-Zhi; Yang, Bo; Zhang, Ji
Organic Preparations and Procedures International, 2013 , vol. 45, # 4 p. 321 - 324
反应条件
1: NaN3 / tetrahydrofuran; H2O / 0 °C 2: toluene / Heating 3: aq. NaOH View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 16, # 22 p. 5864 - 5869
反应条件
diethylenetriamine-N,N,N',N'',N''-pentaacetic acid; ammonia; copper(II) oxide; potassium hydroxide in water T=100°C; 12 h;
参考文献
Yang, Bo; Liao, Lihao; Zeng, Yongheng; Zhu, Xinhai; Wan, Yiqian
Catalysis Communications, 2014 , vol. 45, p. 100 - 103
反应条件
sodium azide; chloroform; sulfuric acid
参考文献
Angewandte Chemie, , vol. 45, p. 536
反应条件
sodium hydroxide in ethanol Heating;
参考文献
Monatshefte fuer Chemie, , vol. 98, p. 1962 - 1972
反应条件
1,4-diaza-bicyclo[2.2.2]octane; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine in methanol Lossen Rearrangement; 3 h; RefluxGreen chemistry;
参考文献
Kreye, Oliver; Wald, Sarah; Meier, Michael A. R.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 1 p. 81 - 86
反应条件
CuSO4‵5H2O; K3PO4*7H2O; water; [14C]-Sucrose in water T=90°C; 15 h; Green chemistry; Catalytic behavior;
参考文献
Huang, Manna; Wang, Leilei; Zhu, Xinhai; Mao, Zuxing; Kuang, Daizhi; Wan, Yiqian
European Journal of Organic Chemistry, 2012 , # 26 p. 4897 - 4901
反应条件
water; potassium carbonate in methanol 20 h; Ambient temperature;
参考文献
Synthesis, , # 1 p. 38 - 40
