1,4-二(4-氯苯基)丁烷-1,4-二酮合成路线 （共 28 条）
参考文献
Campbell; Khanna
Journal of the Chemical Society, 1949 , p. Spl. 33, 35
参考文献
Campbell; Khanna
Journal of the Chemical Society, 1949 , p. Spl. 33, 35
反应条件
1: With lithium hexamethyldisilazane in tetrahydrofuran
T=-78°C; 0.5 h;
2: in tetrahydrofuran
T=-45°C; 3 h; Further stages.;
参考文献
Imachi, Shohei; Mukaiyama, Teruaki
Chemistry Letters, 2007 , vol. 36, # 6 p. 718 - 719
反应条件
sodium carbonate; triethylamine; 3,4-dimethyl-5-(2-hydroxyethyl)-thiazolium iodide in ethanol
T=80°C; 6 h;
参考文献
Stetter, Hermann; Jonas, Friedrich
Chemische Berichte, 1981 , vol. 114, # 2 p. 564 - 580
反应条件
3-(2,4,6-trimethyl-phenyl)-5,6,7,8-tetrahydro-4H-cycloheptathiazol-3-ium perchlorate; potassium tert-butylate in 1,4-dioxane
T=30 - 70°C; Stetter reaction; 22.75 h; Inert atmosphere;
参考文献
Bhunia, Anup; Yetra, Santhivardhana Reddy; Bhojgude, Sachin Suresh; Biju, Akkattu T.
Organic Letters, 2012 , vol. 14, # 11 p. 2830 - 2833
反应条件
indium monobromide in tetrahydrofuran
T=20°C; 24 h;
参考文献
Peppe, Clovis; Pavao Das Chagas, Rafael
Synlett, 2004 , # 7 p. 1187 - 1190
反应条件
tetraethylammonium iodide; zinc; NiBr2(PPh3)2 in tetrahydrofuran
2.5 h; Ambient temperature;
参考文献
Iyoda, Masahiko; Sakaitani, Masahiro; Kojima, Atsuko; Oda, Masaji
Tetrahedron Letters, 1985 , vol. 26, # 31 p. 3719 - 3722
反应条件
iodine; zinc in tetrahydrofuran
16 h; Heating;
参考文献
Ceylan, Mustafa; Guerdere, M. Burcu; Budak, Yakup; Kazaz, Cavit; Secen, Hasan
Synthesis, 2004 , # 11 p. 1750 - 1754
反应条件
oxalic acid in tetrahydrofuran
1.5 h; Heating;
参考文献
Takahashi, Kazumasa; Matsuzaki, Masahiro; Ogura, Katsuyuki; Iida, Hirotada
Journal of Organic Chemistry, 1983 , vol. 48, # 11 p. 1909 - 1912
反应条件
[Ru(tris(2,2'-bipyridyl))3]Cl2·6H2O; potassium carbonate; triethylamine in acetonitrile
T=20°C; 16 h; Schlenk techniqueIrradiation;
参考文献
Xuan, Jun; Feng, Zhu-Jia; Chen, Jia-Rong; Lu, Liang-Qiu; Xiao, Wen-Jing
Chemistry - A European Journal, 2014 , vol. 20, # 11 p. 3045 - 3049
