1,4-二(4-氯苯基)丁烷-1,4-二酮合成路线 (共 28 条)
反应条件
hydroxymethanesulfinic acid sodium salt in ethanol
1 h; Heating;
参考文献
Harris, Alan R.
Synthetic Communications, 1987 , vol. 17, # 13 p. 1587 - 1592
反应条件
aluminum isopropoxide; isopropyl alcohol
参考文献
Lutz; Gillespie
Journal of the American Chemical Society, 1950 , vol. 72, p. 344
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Campbell; Khanna
Nature (London, United Kingdom), 1948 , vol. 161, p. 54
反应条件
indium monobromide in tetrahydrofuran
T=20°C; 24 h; Title compound not separated from byproducts;
参考文献
Peppe, Clovis; Pavao Das Chagas, Rafael
Synlett, 2004 , # 7 p. 1187 - 1190
反应条件
2: 78 percent / 30percent aq. oxalic acid / tetrahydrofuran / 1.5 h / Heating
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参考文献
Takahashi, Kazumasa; Matsuzaki, Masahiro; Ogura, Katsuyuki; Iida, Hirotada
Journal of Organic Chemistry, 1983 , vol. 48, # 11 p. 1909 - 1912
反应条件
methyloxirane in water; acetonitrile
4 h; Irradiation;
参考文献
Dhavale, Dilip D.; Mali, Vasant P.; Sudrik, Surendra G.; Sonawane, Harikisan R.
Tetrahedron, 1997 , vol. 53, # 49 p. 16789 - 16794
反应条件
methanol; Woollins’ reagent
T=20°C; 1.5 h; chemoselective reaction;
参考文献
Mandal, Madhumita; Chatterjee, Sourav; Jaisankar, Parasuraman
Synlett, 2012 , vol. 23, # 18 p. 2615 - 2618,4
反应条件
in methanol
21 h; Irradiation; Product distributionMechanism;
参考文献
Arora, Kanwar J. S.; Collier, John R.; Deodhar, Dinker J.; Hesabi, Masoud-M.; Hill, John
Journal of Chemical Research, Miniprint, 1985 , # 6 p. 2148 - 2183
反应条件
in benzene
4.5 h; Irradiationother solvents, various irradiation sources; in the presence of maleic anhydride; Product distributionMechanism;
参考文献
Arora, Kanwar J. S.; Collier, John R.; Deodhar, Dinker J.; Hesabi, Masoud-M.; Hill, John
Journal of Chemical Research, Miniprint, 1985 , # 6 p. 2148 - 2183