4-甲氧基苄基对茴香酸酯合成路线 (共 22 条)
反应条件
2,4,6-trimethyl-pyridine; hydrogen; chlorohydridotris(triphenylphosphine)ruthenium in toluene T=55°C; P=760 Torr; 19 h;
参考文献
Grushin, Vladimir V.; Alper, Howard
Journal of Organic Chemistry, 1991 , vol. 56, # 17 p. 5159 - 5161
反应条件
potassium carbonate; butanone; amino alcohol-based Ir bifunctional catalyst T=20°C; 26 h;
参考文献
Suzuki, Takeyuki; Matsuo, Tomohito; Watanabe, Kazuhiro; Katoh, Tadashi
Synlett, 2005 , # 9 art. no. U05305ST, p. 1453 - 1455
反应条件
1: (4-methoxyphenyl)methanol With triethylamine in dichloromethane 0.166667 h; 2: 4-methoxy-benzoyl chloride in dichloromethane T=20°C; 2 h; 3: in dichloromethane T=45°C;
参考文献
Rolfe, Alan; Loh, Joanna K.; Maity, Pradip K.; Hanson, Paul R.
Organic Letters, 2011 , vol. 13, # 1 p. 4 - 7
反应条件
iodine; potassium carbonate in tert-butyl alcohol T=20°C; 31 h;
参考文献
Oded, Kobi; Musa, Sanaa; Gelman, Dmitri; Blum, Jochanan
Catalysis Communications, 2012 , vol. 20, p. 68 - 70
反应条件
in dichloromethane T=20°C; 24 h; Inert atmosphere;
参考文献
Shah, Jigisha P.; Russo, Christopher M.; Howard, Kyle T.; Chisholm, John D.
Tetrahedron Letters, 2014 , vol. 55, # 10 p. 1740 - 1742
反应条件
sodium hydride Tishchenko reaction; 16 h; Neat (no solvent)High speed ball milling;
参考文献
Rajesh, Kunjanpillai; Berke, Heinz
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 5 p. 901 - 906
反应条件
La[N(TMS)2]3 in benzene-d6 T=25°C; 24 h;
参考文献
Seo, SungYong; Marks, Tobin J.
Organic Letters, 2008 , vol. 10, # 2 p. 317 - 319
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in water T=80°C; 6 h;
参考文献
Majji, Ganesh; Guin, Srimanta; Gogoi, Anupal; Rout, Saroj Kumar; Patel, Bhisma K.
Chemical Communications, 2013 , vol. 49, # 29 p. 3031 - 3033
反应条件
2,6-dimethylpyridine; lithium perchlorate; 2-(4-bromophenyl)-1-methyl-4,5-diphenyl-1H-imidazole in dichloromethane; water; acetonitrile Electrolysis;
参考文献
Zeng, Cheng-Chu; Zhang, Ni-Tao; Lam, Chiu Marco; Little, R. Daniel
Organic Letters, 2012 , vol. 14, # 5 p. 1314 - 1317
反应条件
trimethylamine borane in xylene 9 h; Heating;
参考文献
Trapani, Giuseppe; Reho, Antonia; Latrofa, Andrea; Liso, Gaetano
Synthesis, 1990 , # 9 p. 853 - 854