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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
9-芴甲醇
合成路线
（共 77 条）
190431-89-1
→
反应条件
24324-17-2
9-芴甲醇
+
502897-85-0
9-(氟甲基)-9H-芴
反应条件
perchloric acid; water; NAF T=70°C; nucleophilic selectivities expressed as ratio od second-order rate constants for reaction of title comp. kNu/kHOH;
参考文献
Journal of the American Chemical Society, , vol. 119, # 21 p. 4834 - 4840
190431-89-1
→
反应条件
24324-17-2
9-芴甲醇
反应条件
sodium azide; perchloric acid; water T=70°C; nucleophilic selectivities expressed as ratio od second-order rate constants for reaction of title comp. kNu/kHOH;
参考文献
Journal of the American Chemical Society, , vol. 119, # 21 p. 4834 - 4840
86-73-7
芴
+
109-94-4
甲酸乙酯
→
反应条件
24324-17-2
9-芴甲醇
反应条件
sodium tetrahydroborate; sodium hydride 1.) ether, reflux, 10h; 2.) methanol, room temp., 2 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 45, # 21 p. 4250 - 4252
67-56-1
甲醇
+
190431-89-1
→
反应条件
24324-17-2
9-芴甲醇
反应条件
perchloric acid; water T=70°C; nucleophilic selectivities expressed as ratio od second-order rate constants for reaction of title comp. kNu/kHOH;
参考文献
Journal of the American Chemical Society, , vol. 119, # 21 p. 4834 - 4840
75-89-8
2,2,2-三氟乙醇
+
190431-89-1
→
反应条件
24324-17-2
9-芴甲醇
反应条件
perchloric acid; water T=70°C; nucleophilic selectivities expressed as ratio od second-order rate constants for reaction of title comp. kNu/kHOH;
参考文献
Journal of the American Chemical Society, , vol. 119, # 21 p. 4834 - 4840
540-72-7
硫氰酸钠
+
190431-89-1
→
反应条件
24324-17-2
9-芴甲醇
反应条件
perchloric acid; water T=70°C; nucleophilic selectivities expressed as ratio od second-order rate constants for reaction of title comp. kNu/kHOH;
参考文献
Journal of the American Chemical Society, , vol. 119, # 21 p. 4834 - 4840
127-09-3
乙酸钠
+
190431-89-1
→
反应条件
24324-17-2
9-芴甲醇
+
63839-86-1
反应条件
perchloric acid; water T=70°C; nucleophilic selectivities expressed as ratio od second-order rate constants for reaction of title comp. kNu/kHOH;
参考文献
Journal of the American Chemical Society, , vol. 119, # 21 p. 4834 - 4840
75-05-8
乙腈
+
190431-89-1
→
反应条件
24324-17-2
9-芴甲醇
反应条件
perchloric acid; water T=70°C; nucleophilic selectivities expressed as ratio od second-order rate constants for reaction of title comp. kNu/kHOH;
参考文献
Journal of the American Chemical Society, , vol. 119, # 21 p. 4834 - 4840
67-56-1
甲醇
+
56954-81-5
→
反应条件
4425-82-5
9-亚甲基芴
+
24324-17-2
9-芴甲醇
反应条件
water; sodium methylate T=25°C; Rate constantMechanism;
参考文献
Journal of the American Chemical Society, , vol. 119, # 21 p. 4834 - 4840
67-56-1
甲醇
+
190431-89-1
→
反应条件
4425-82-5
9-亚甲基芴
+
24324-17-2
9-芴甲醇
反应条件
water; sodium methylate T=25°C; Rate constantMechanism;
参考文献
Journal of the American Chemical Society, , vol. 119, # 21 p. 4834 - 4840
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