1,1,2-三甲氧基乙烷合成路线 （共 14 条）
反应条件
hydrogenchloride T=50°C; ΔE(excit.); Rate constantKineticsMechanism;
参考文献
Carbohydrate Research, , vol. 87, p. 35 - 50
反应条件
1: 2-methoxyacetaldehyde dimethyl acetal With hydrogenchloride in water
T=50°C; 1.5 h;
2: 4-(2-piperazin-1-yl-thiazol-4-yl)-benzoic acid With sodium acetate; acetic acid in water; acetonitrile
T=20°C; pH=5.5; 1.5 h;
3: With sodium cyanoborohydride in water; acetonitrile
T=20°C; 16 h;
参考文献
MEDIVIR AB
Patent: WO2007/6714 A1, 2007 ;
Location in patent: Page/Page column 90 ;
反应条件
toluene-4-sulfonic acid
Substitution; Heating;
参考文献
Taskinen, Esko
Magnetic Resonance in Chemistry, 1998 , vol. 36, # 8 p. 573 - 578
反应条件
potassium dichromate; acetic acid
1) H2O, EtOH, 60 deg C, 20 h; 2) heating, 3 min; Yield given. Multistep reaction;
参考文献
Mitsunaga, Katsuyoshi; Koike, Kazuo; Tanaka, Tomoko; Ohkawa, Youko; Kobayashi, Yuko; et al.
Phytochemistry (Elsevier), 1994 , vol. 35, # 3 p. 799 - 802
