亚甲基双[二甲基(2-吡啶基)硅烷]合成路线 （共 2 条）
反应条件
1: (pyridin-2-yl)trimethylsilane With tert.-butyl lithium in diethyl ether; pentane T=-78°C; Metallation; 0.5 h; 2: (2-pyridyl)Me2SiH in diethyl ether; pentane T=-78°C; Substitution;
参考文献
Itami; Kamei; Mitsudo; Nokami; Yoshida
Journal of Organic Chemistry, 2001 , vol. 66, # 11 p. 3970 - 3976
反应条件
1: (pyridin-2-yl)trimethylsilane With tert.-butyl lithium in diethyl ether; pentane T=-78°C; Metallation; 0.5 h; 2: (pyridin-2-yl)trimethylsilane in diethyl ether; pentane T=-78°C; Substitution; 1 h; Further stages.;
参考文献
Itami, Kenichiro; Nokami, Toshiki; Yoshida, Jun-Ichi
Organic Letters, 2000 , vol. 2, # 9 p. 1299 - 1302
