3,7-二甲基-1,6-辛二烯合成路线 (共 77 条)
反应条件
triethylamine in tetrahydrofuran T=50°C; 8 h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 36, p. 1455 - 1461
反应条件
triethylamine in tetrahydrofuran T=50°C; 8 h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 36, p. 1455 - 1461
反应条件
methanol; barium 1.) THF, -75 deg C, 30 min, 2.) THF, 5 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 116, # 14 p. 6130 - 6141
反应条件
hydrogen in toluene T=100°C; 12 h; chemoselective reaction;
参考文献
Chemical Communications, , vol. 48, # 53 p. 6723 - 6725
反应条件
triethylamine in n-heptane Irradiation;
参考文献
Tetrahedron, , vol. 32, p. 1391 - 1393
反应条件
sodium cyanoborohydride; triphenylphosphine; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=66°C; 48 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 21, p. 27 - 30
反应条件
1: Li / tetrahydrofuran / -5 °C 2: 80 percent / (AcOH)2*BF3 / -25 °C / 1 equivalent (AcOH)2*BF3 View Scheme
参考文献
Tetrahedron Letters, , vol. 21, p. 4267 - 4270
反应条件
samarium diiodide; isopropyl alcohol; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 2 h; Heating; Yield given. Title compound not separated from byproducts;
参考文献
Tabuchi, Takanori; Inanaga, Junji; Yamaguchi, Masaru
Tetrahedron Letters, 1986 , vol. 27, # 5 p. 601 - 602
反应条件
Pd(dibenzylidene acetone)3*CHCl3; tributylphosphine in 1,4-dioxane 2 h; Heating;
参考文献
Tsuji, Jiro; Shimizu, Isao; Minami, Ichiro
Chemistry Letters, 1984 , p. 1017 - 1020
反应条件
samarium diiodide; tert-butyl alcohol in tetrahydrofuran 4 h;
参考文献
Tetrahedron Letters, , vol. 39, # 13 p. 1777 - 1780