7-噁双环[2.2.l]-5-庚烯合成路线 (共 5 条)
反应条件
2-bromobenzene boronic acid in dichloromethane T=25°C; 48 h;
参考文献
Al-Zoubi, Raed M.; Marion, Olivier; Hall, Dennis G.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 15 p. 2876 - 2879
反应条件
in dichloromethane T=27°C; P=15001200 Torr; 4 h; Yields of byproduct given;
参考文献
Hamada, Manabu; Inami, Yoshikazu; Nagai, Yasuhito; Higashi, Toshinori; Shoji, Mitsuru; Ogawa, Seiichiro; Umezawa, Kazuo; Sugai, Takeshi
Tetrahedron Asymmetry, 2009 , vol. 20, # 18 p. 2105 - 2111
反应条件
sodium hydroxide; water 20 h; Ambient temperature;
参考文献
Tran, Chuong Hao; Crout, David H. G.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 6 p. 1065 - 1068
反应条件
1: With sodium hydroxide in water 2: With hydrogenchloride in water optical yield given as percent de;
参考文献
Di Bussolo, Valeria; Frau, Ileana; Checchia, Lorenzo; Favero, Lucilla; Pineschi, Mauro; Uccello-Barretta, Gloria; Balzano, Federica; Roselli, Graziella; Renzi, Gabriele; Crotti, Paolo
Tetrahedron, 2011 , vol. 67, # 25 p. 4696 - 4709
反应条件
water in ethanol T=37°C; pig liver esterase, pH 7.5; kinetic constants of enzymatic hydrolyse;
参考文献
Sicsic, Sames; Leroy, Jacques; Wakselman, Claude
Synthesis, 1987 , # 2 p. 155 - 156