2-[(2-甲基-2-丙基)二硫基]吡啶合成路线 (共 49 条)
反应条件
n-hexadecanoyl chloride in benzene
T=80°C; 3 h;
参考文献
Barton, Derek H. R.; Crich, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1613 - 1620
反应条件
Na salt of N-hydroxypyridine-2-thione in chlorobenzene
0.75 h; Heating;
参考文献
Barton, Derek H. R.; Crich, David
Tetrahedron Letters, 1984 , vol. 25, # 26 p. 2787 - 2790
反应条件
n-hexadecanoyl chloride in benzene
T=80°C; 4.5 h;
参考文献
Barton, Derek H. R.; Crich, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1613 - 1620
反应条件
Fonderma in chlorobenzene
Heating;
参考文献
Barton, Derek H.R.; Crich, David
Tetrahedron Letters, 1985 , vol. 26, # 6 p. 757 - 760
反应条件
Na salt of N-hydroxypyridine-2-thione in chlorobenzene
0.5 h; Heating;
参考文献
Barton, Derek H. R.; Crich, David
Tetrahedron Letters, 1984 , vol. 25, # 26 p. 2787 - 2790
反应条件
Na salt of N-hydroxypyridine-2-thione in chlorobenzene
0.5 h; Heating;
参考文献
Barton, Derek H. R.; Crich, David
Tetrahedron Letters, 1984 , vol. 25, # 26 p. 2787 - 2790
反应条件
in dichloromethane
T=0 - 5°C; 0.5 h; Irradiation;
参考文献
Barton, Derek H. R.; Fontana, Giovanni
Synthetic Communications, 1996 , vol. 26, # 10 p. 1953 - 1968
反应条件
oxygen; 2-methylpropane-2-thiol in toluene
T=80°C; 1 h; adding 15 min; Yields of byproduct given;
参考文献
Barton, Derek H. R.; Crich, David; Motherwell, William B.
Tetrahedron, 1985 , vol. 41, # 19 p. 3901 - 3924
反应条件
4-(N,N-dimethlyamino)pyridine; n-hexadecanoyl chloride in toluene
T=110°C; 2.5 h;
参考文献
Barton, Derek H. R.; Crich, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1613 - 1620
反应条件
4-(N,N-dimethlyamino)pyridine; dimethyl-2,2 thia-3 hexene-5 in toluene
T=110°C; 2.5 h;
参考文献
Barton, Derek H. R.; Crich, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1613 - 1620