1,3,5-苯三酚三乙醚合成路线 （共 15 条）
反应条件
potassium hydroxide; MeO(CH2CH2O)nMe (M 500) in water
1 h; Heating;
参考文献
Kirillova, K. M.; Skvortsova, T. A.; Nikonova, L. Z.; Chugunov, Yu. V.; Igonin, V. B.; Mukhtarov, A. Sh.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 3.1 p. 427 - 430
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 3 p. 527 - 530
参考文献
Johnson; Barnes; McElvain
Journal of the American Chemical Society, 1940 , vol. 62, p. 964,968, 971
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McElvain; Langston
Journal of the American Chemical Society, 1943 , vol. 65, p. 2239,2240
反应条件
bis(1,5-cyclooctadiene)nickel (0); triphenylphosphine in tetrahydrofuran
T=80°C; 20 h;
参考文献
Tsuda, Tetsuo; Kunisada, Kazuhiro; Nagahama, Norio; Morikawa, Shonei; Saegusa, Takeo
Synthetic Communications, 1989 , vol. 19, # 9-10 p. 1575 - 1582
反应条件
bis(1,5-cyclooctadiene)nickel (0); tri-cyclo-hexyl-phosphine in tetrahydrofuran
T=80°C; 20 h;
参考文献
Tsuda, Tetsuo; Kunisada, Kazuhiro; Nagahama, Norio; Morikawa, Shonei; Saegusa, Takeo
Synthetic Communications, 1989 , vol. 19, # 9-10 p. 1575 - 1582
反应条件
di[(2,4-bis-tert-butyl-1-methoxy-3-neopentylcyclopentadienyl)dichlororuthenium(III)] in dichloromethane
T=60°C; 8 h; regioselective reaction;
参考文献
Dutta, Barnali; Curchod, Basile F. E.; Campomanes, Pablo; Solari, Euro; Scopelliti, Rosario; Rothlisberger, Ursula; Severin, Kay
Chemistry - A European Journal, 2010 , vol. 16, # 28 p. 8400 - 8409
反应条件
1: HCl (g) / 6 h / Heating
2: 92 percent / KOH, MeO(CH2CH2O)nMe (M 500) / H2O / 1 h / Heating
View Scheme
参考文献
Kirillova, K. M.; Skvortsova, T. A.; Nikonova, L. Z.; Chugunov, Yu. V.; Igonin, V. B.; Mukhtarov, A. Sh.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 3.1 p. 427 - 430
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 3 p. 527 - 530
反应条件
bis(1,5-cyclooctadiene)nickel (0); diethylphosphinoethane in tetrahydrofuran
T=80°C; 20 h;
参考文献
Tsuda, Tetsuo; Kunisada, Kazuhiro; Nagahama, Norio; Morikawa, Shonei; Saegusa, Takeo
Synthetic Communications, 1989 , vol. 19, # 9-10 p. 1575 - 1582
反应条件
1: hydrochloric acid
2: KOH; alcohol
View Scheme
参考文献
Will; Albrecht
Chemische Berichte, 1884 , vol. 17, p. 2103
参考文献
Bredereck et al.
Chemische Berichte, 1953 , vol. 86, p. 1085,1093
反应条件
potassium hydroxide; ethanol
参考文献
Will; Albrecht
Chemische Berichte, 1884 , vol. 17, p. 2103
