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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯硼酸频哪醇酯
合成路线
（共 245 条）
76-09-5
频哪醇
+
1201-45-2
→
反应条件
24388-23-6
苯硼酸频哪醇酯
反应条件
24 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 38, # 19 p. 3447 - 3450
626-39-1
1,3,5-三溴苯
+
24388-23-6
苯硼酸频哪醇酯
→
反应条件
103068-20-8
5'-溴间三联苯
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in tetrahydrofuran; water T=65°C; 5 h; Inert atmosphere;
参考文献
Kim, Soo-Kang; Yang, Bing; Ma, Yuguang; Lee, Ji-Hoon; Park, Jong-Wook
Journal of Materials Chemistry, 2008 , vol. 18, # 28 p. 3376 - 3384
1072-97-5
2-氨基-5-溴吡啶
+
24388-23-6
苯硼酸频哪醇酯
→
反应条件
33421-40-8
2-氨基-5-苯基吡啶
反应条件
potassium phosphate; (C5H5FeC5H3C(CH3)NC6H4CH3)PdCl(tricyclohexylphosphine); potassium acetate in 1,4-dioxane; water T=100°C; Suzuki coupling; 15 h; Inert atmosphere;
参考文献
Wang, Lianhui; Cui, Xiuling; Li, Jingya; Wu, Yusheng; Zhu, Zhiwu; Wu, Yangjie
European Journal of Organic Chemistry, 2012 , # 3 p. 595 - 603
24388-23-6
苯硼酸频哪醇酯
→
反应条件
3073-05-0
反应条件
1.1: palladium diacetate; potassium carbonate; triphenylphosphine / tetrahydrofuran; water / 18 h / Reflux 2.1: water; potassium hydroxide / ethylene glycol / 2 h / Reflux 3.1: sodium hydroxide; potassium hexacyanoferrate(III) / tetrahydrofuran; ethylene glycol / 3 h 3.2: pH 3 View Scheme
参考文献
Davis, Matthew C.; Groshens, Thomas J.
Synthetic Communications, 2011 , vol. 41, # 2 p. 206 - 218
3430-13-5
+
24388-23-6
苯硼酸频哪醇酯
→
反应条件
3256-88-0
反应条件
potassium phosphate; (C5H5FeC5H3C(CH3)NC6H4CH3)PdCl(tricyclohexylphosphine); potassium acetate in 1,4-dioxane; water T=100°C; Suzuki coupling; 15 h; Inert atmosphere;
参考文献
Wang, Lianhui; Cui, Xiuling; Li, Jingya; Wu, Yusheng; Zhu, Zhiwu; Wu, Yangjie
European Journal of Organic Chemistry, 2012 , # 3 p. 595 - 603
373-53-5
+
24388-23-6
苯硼酸频哪醇酯
→
反应条件
350-50-5
反应条件
potassium carbonate; tris-(dibenzylideneacetone)dipalladium(0); tris-(o-tolyl)phosphine in N,N-dimethyl-formamide T=60°C; 0.0833333 h; Product distribution / selectivity;
参考文献
Gifu University; Riken; Hamamatsu Photonics K.K.
Patent: EP2070897 A1, 2009 ;
Location in patent: Page/Page column 11-12 ;
626-05-1
+
24388-23-6
苯硼酸频哪醇酯
→
反应条件
39774-26-0
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in water; toluene Suzuki coupling; 24 h; Heating;
参考文献
Jin, Ri-Zhe; Bian, Zheng; Kang, Chuan-Qing; Guo, Hai-Quan; Gao, Lian-Xun
Synthetic Communications, 2005 , vol. 35, # 14 p. 1897 - 1902
73583-37-6
+
24388-23-6
苯硼酸频哪醇酯
→
反应条件
42260-39-9
反应条件
potassium phosphate; (C5H5FeC5H3C(CH3)NC6H4CH3)PdCl(tricyclohexylphosphine); potassium acetate in 1,4-dioxane; water T=100°C; Suzuki coupling; 15 h; Inert atmosphere;
参考文献
Wang, Lianhui; Cui, Xiuling; Li, Jingya; Wu, Yusheng; Zhu, Zhiwu; Wu, Yangjie
European Journal of Organic Chemistry, 2012 , # 3 p. 595 - 603
24388-23-6
苯硼酸频哪醇酯
+
38749-79-0
→
反应条件
3256-89-1
反应条件
potassium phosphate; (C5H5FeC5H3C(CH3)NC6H4CH3)PdCl(tricyclohexylphosphine); potassium acetate in 1,4-dioxane; water T=100°C; Suzuki coupling; 6 h; Inert atmosphere;
参考文献
Wang, Lianhui; Cui, Xiuling; Li, Jingya; Wu, Yusheng; Zhu, Zhiwu; Wu, Yangjie
European Journal of Organic Chemistry, 2012 , # 3 p. 595 - 603
24388-23-6
苯硼酸频哪醇酯
→
反应条件
5002-26-6
反应条件
cesium fluoride; Na2[PdCl4] in methanol T=40°C; Arylation; cross-coupling; 24 h;
参考文献
Willis; Strongin
Tetrahedron Letters, 2000 , vol. 41, # 33 p. 6271 - 6274
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