(2E)-3-(4-硝基苯基)-2-丙烯酸乙酯合成路线 （共 77 条）
反应条件
Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 19 p. 1424 - 1426
反应条件
2,3-dimethylbutane-2,3-diol; [MoO2Cl2(dmf)2] in toluene T=150°C; 0.333333 h; Microwave irradiation; chemoselective reaction;
参考文献
Garcia, Nuria; Garcia-Garcia, Patricia; Fernandez-Rodriguez, Manuel A.; Rubio, Ruben; Pedrosa, Maria R.; Arnaiz, Francisco J.; Sanz, Roberto
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 2-3 p. 321 - 327
反应条件
PdI2(N-methylbenzothiazolylidene)2; tetra-n-butylammonium acetate in various solvent(s) T=130°C; Heck arylation; 4.5 h;
参考文献
Calo, Vincenzo; Nacci, Angelo; Monopoli, Antonio; Laera, Stefania; Cioffi, Nicola
Journal of Organic Chemistry, 2003 , vol. 68, # 7 p. 2929 - 2933
参考文献
van der Lee
Recueil des Travaux Chimiques des Pays-Bas, 1929 , vol. 48, p. 1139
Full Text Show Details
Guastalla
Atti della Accademia delle Scienze di Torino, Classe di Scienze Fisiche, Matematiche e Naturali, vol. 63, p. 130
Chem. Zentralbl., 1928 , vol. 99, # II p. 984
反应条件
1.1: 98 percent / AD-mix-β 2.1: Bu2SnO / 1,2-dichloro-ethane / 24 h / Heating 2.2: 6 h / Heating 2.3: 62 percent / Bu4NBr / 6 h / Heating 3.1: 80 percent / Ti(OiPr)4 / ethanol 4.1: 92 percent / NaBH4 5.1: 92 percent / NaOH View Scheme
参考文献
Park, Jung Nam; Ko, Soo Y.; Koh, Hun Y.
Tetrahedron Letters, 2000 , vol. 41, # 29 p. 5553 - 5556
反应条件
hydrogenchloride; sodium hydroxide in 1,4-dioxane
参考文献
Meiji Seika Kaisha Ltd.
Patent: US6576627 B1, 2003 ;
反应条件
1.1: 98 percent / AD-mix-β 2.1: Bu2SnO / 1,2-dichloro-ethane / 24 h / Heating 2.2: 6 h / Heating 2.3: 62 percent / Bu4NBr / 6 h / Heating 3.1: 80 percent / Ti(OiPr)4 / ethanol 4.1: 92 percent / NaBH4 5.1: 92 percent / NaOH View Scheme
参考文献
Park, Jung Nam; Ko, Soo Y.; Koh, Hun Y.
Tetrahedron Letters, 2000 , vol. 41, # 29 p. 5553 - 5556
反应条件
1.1: 98 percent / AD-mix-β 2.1: Bu2SnO / 1,2-dichloro-ethane / 24 h / Heating 2.2: 6 h / Heating 2.3: 62 percent / Bu4NBr / 6 h / Heating 3.1: 80 percent / Ti(OiPr)4 / ethanol 4.1: 92 percent / NaBH4 5.1: 92 percent / NaOH 6.1: 74 percent View Scheme
参考文献
Park, Jung Nam; Ko, Soo Y.; Koh, Hun Y.
Tetrahedron Letters, 2000 , vol. 41, # 29 p. 5553 - 5556
反应条件
1: pyridinium hydrobromide perbromide / acetic acid 2: 1.) KOtBu, 2.) esterification / 1.) ethanol, 70 deg C View Scheme
参考文献
Butt, G.; Topsom, R. D.
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, 1982 , vol. 38, # 6 p. 649 - 654
反应条件
1.1: 98 percent / AD-mix-β 2.1: Bu2SnO / 1,2-dichloro-ethane / 24 h / Heating 2.2: 6 h / Heating 2.3: 62 percent / Bu4NBr / 6 h / Heating 3.1: 80 percent / Ti(OiPr)4 / ethanol 4.1: 92 percent / NaBH4 5.1: 92 percent / NaOH View Scheme
参考文献
Park, Jung Nam; Ko, Soo Y.; Koh, Hun Y.
Tetrahedron Letters, 2000 , vol. 41, # 29 p. 5553 - 5556
