(2E)-3-(4-硝基苯基)-2-丙烯酸乙酯合成路线 （共 77 条）
参考文献
Monatshefte fuer Chemie, , vol. 68, p. 326,346
反应条件
1: diisobutylaluminium hydride / dichloromethane / -78 °C 2: Cu(ClO4)2*6H2O; trimethylsilylazide; 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,2-dichloro-ethane / 4 h / 60 °C View Scheme
参考文献
Rokade, Balaji V.; Malekar, Sanjeev K.; Prabhu, Kandikere Ramaiah
Chemical Communications, 2012 , vol. 48, # 44 p. 5506 - 5508
反应条件
1: With diisobutylaluminium hydride in tetrahydrofuran; toluene T=-78°C; 1.5 h; 2: With hydrogenchloride in tetrahydrofuran; water; toluene
参考文献
Sato, Masakazu; Kakinuma, Hiroyuki; Amada, Hideaki
Patent: US2006/4078 A1, 2006 ;
Location in patent: Page/Page column 7 ;
反应条件
triethylamine; sulfilimine based palladacycle in 1-methyl-pyrrolidin-2-one
T=140°C; Heck reaction; 12 h;
参考文献
Liu, Xiang; Mao, Yang; Lu, Ming
Applied Organometallic Chemistry, 2012 , vol. 26, # 6 p. 305 - 309
反应条件
PEG-OCOCH2CH2CO2CH2CH2-supported 3-methyl-imidazolium*Cl; potassium carbonate; palladium diacetate
T=160°C; Heck reaction; 48 h;
参考文献
Wang, Liang; Zhang, Yuhong; Xie, Chunsong; Wang, Yanguang
Synlett, 2005 , # 12 art. no. U05205ST, p. 1861 - 1864
反应条件
Rasta resin-PPh3-NBniPr2 in dichloromethane
T=20°C; Wittig reaction; 19 h; Molecular sieve; optical yield given as percent de;
参考文献
Teng, Yan; Lu, Jinni; Toy, Patrick H.
Chemistry - An Asian Journal, 2012 , vol. 7, # 2 p. 351 - 359
反应条件
2C32H12BF24(1-)*C36H36Br2N8O4Ru2(2+); triphenylphosphine in toluene
T=25°C; 2 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Saha, Biswajit; Rahaman, S. M. Wahidur; Sinha, Arup; Bera, Jitendra K.
Australian Journal of Chemistry, 2011 , vol. 64, # 5 p. 583 - 589
反应条件
tributyl-amine; palladium diacetate in xylene
T=120°C; 1 h;
参考文献
Blaser, Hans-Ulrich; Spencer, Alwyn
Journal of Organometallic Chemistry, 1982 , vol. 233, # 2 p. 267 - 274
反应条件
triethylamine; {[Pd(η5-C5H5)Fe(η5-C5H3)C(CH3)=N(C6H4CH3-4)](μ-I)}2 in 1,4-dioxane
T=100°C; 10 h;
参考文献
Wu, Yangjie; Hou, Jianjun; Yun, Hongying; Cui, Xiuling; Yuan, Ruijuan
Journal of Organometallic Chemistry, 2001 , vol. 637-639, p. 793 - 795
反应条件
1,3-bis(2,4,6-trimethylphenyl)imidazolinium chloride; triethylamine in tetrahydrofuran
T=60°C; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Wang, Xiang-Bo; Zou, Xiao-Lei; Du, Guang-Fen; Liu, Zhi-Yong; Dai, Bin
Tetrahedron, 2012 , vol. 68, # 32 p. 6498 - 6503
