(2E)-3-(4-硝基苯基)-2-丙烯酸乙酯合成路线 (共 77 条)
反应条件
palladium diacetate in ethanol; water
T=20°C; Heck arylation; 0.5 h;
参考文献
Artuso, Emma; Barbero, Margherita; Degani, Iacopo; Dughera, Stefano; Fochi, Rita
Tetrahedron, 2006 , vol. 62, # 13 p. 3146 - 3157
反应条件
Verkade nonionic superbase in tetrahydrofuran
T=20°C; 0.5 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Chintareddy, Venkat Reddy; Ellern, Arkady; Verkade, John G.
Journal of Organic Chemistry, 2010 , vol. 75, # 21 p. 7166 - 7174
反应条件
potassium carbonate; 18-crown-6 ether in acetonitrile
T=80°C; 2 h;
参考文献
Makosza, M.; Tyrala, A.
Synthesis, 1987 , # 12 p. 1142 - 1144
参考文献
Meiji Seika Kaisha Ltd.
Patent: US6576627 B1, 2003 ;
反应条件
pyrrolidine; 5 palladium on charcoal; tetrabutylammomium bromide; oxygen in 1-methyl-pyrrolidin-2-one
T=80°C; Heck Reaction; P=2587.76 Torr; 10 h;
参考文献
Dighe, Mahesh G.; Lonkar, Sachin L.; Degani, Mariam S.
Synlett, 2013 , vol. 24, # 3 art. no. ST-2012-D0969-L, p. 347 - 350
反应条件
potassium carbonate in ethanol
Wittig Olefination; Milling; diastereoselective reaction;
参考文献
Shearouse, William C.; MacK, James
Green Chemistry, 2012 , vol. 14, # 10 p. 2771 - 2775,5
反应条件
poly{styrene-co-[4-(N-methyl-N-vinylbenzyl-amino)pyridine]-co-[1-phenyl-3-(4-vinylbenzyl)piperazine]} in N,N-dimethyl-formamide
T=50°C; decarboxylative Doebner-Knoevenagel condensation reaction; optical yield given as percent destereoselective reaction;
参考文献
Lu, Jinni; Toy, Patrick H.
Synlett, 2011 , # 12 p. 1723 - 1726
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane
T=20°C; 16 h;
参考文献
Blakemore, Paul R.; Ho, Danny K.H.; Nap, W. Mieke
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 8 p. 1365 - 1368
反应条件
lanthanum trifluoromethanesulphonate in dichloromethane
T=20°C; 8 h;
参考文献
Qian, Changtao; Wang, Longcheng
Tetrahedron, 2000 , vol. 56, # 37 p. 7193 - 7197
反应条件
PEG-OCOCH2CH2CO2CH2CH2-supported 3-methyl-imidazolium*Cl; potassium carbonate; palladium diacetate
T=140°C; Heck reaction; 8 h;
参考文献
Wang, Liang; Zhang, Yuhong; Xie, Chunsong; Wang, Yanguang
Synlett, 2005 , # 12 art. no. U05205ST, p. 1861 - 1864