(2E)-3-(4-硝基苯基)-2-丙烯酸乙酯合成路线 （共 77 条）
反应条件
palladium diacetate in ethanol; water
T=20 - 25°C; Heck arylation; 0.25 h;
参考文献
Artuso, Emma; Barbero, Margherita; Degani, Iacopo; Dughera, Stefano; Fochi, Rita
Tetrahedron, 2006 , vol. 62, # 13 p. 3146 - 3157
反应条件
sodium hydroxide in dichloromethane; water
T=25°C; Wittig reaction; Sonication; stereoselective reaction;
参考文献
Riccaboni, Mauro; La Porta, Elena; Martorana, Andrea; Attanasio, Roberta
Tetrahedron, 2010 , vol. 66, # 23 p. 4032 - 4039
反应条件
bis(η3-allyl-μ-chloropalladium(II)); oxygen; copper(l) chloride in acetonitrile
T=70°C; P=760.051 Torr; 5 h; Schlenk techniqueMolecular sieve; regioselective reaction;
参考文献
Su, Yu-Han; Wu, Zhao; Tian, Shi-Kai
Chemical Communications, 2013 , vol. 49, # 58 p. 6528 - 6530
反应条件
1: ethyl(diphenylphosphoryl)acetate With potassium tert-butylate in dimethyl sulfoxide
2: 4-nitrobenzaldehdye in dimethyl sulfoxide
T=20°C; 0.5 h;
参考文献
Appel, Roland; Loos, Robert; Mayr, Herbert
Journal of the American Chemical Society, 2009 , vol. 131, # 2 p. 704 - 714
反应条件
triethylamine in acetonitrile
T=80°C; Horner-Wadsworth-Emmons reaction; P=6000480 Torr; 72 h;
参考文献
Has-Becker; Bodmann; Kreuder; Santoni; Rein; Reiser
Synlett, 2001 , # 9 p. 1395 - 1398
反应条件
4-(N,N-dimethlyamino)pyridine; 1,3-bis(2,4,6-trimethylphenyl)imidazolinium chloride in toluene
T=60°C; 2 h;
参考文献
Zeitler, Kirsten
Organic Letters, 2006 , vol. 8, # 4 p. 637 - 640
反应条件
Mg/La mixed oxide in N,N-dimethyl-formamide
T=20°C; Wittig reaction; optical yield given as percent destereoselective reaction;
参考文献
Kantam, M. Lakshmi; Kumar, K.B. Shiva; Balasubramanyam; Venkanna; Figueras
Journal of Molecular Catalysis A: Chemical, 2010 , vol. 321, # 1-2 p. 10 - 14
反应条件
AlCl3, aluminium chloride; Oxonereg; in water
T=20°C; Wittig reaction; 2 h; stereoselective reaction;
参考文献
Wu, Shang; Ma, Hengchang; Lei, Ziqiang
Tetrahedron, 2010 , vol. 66, # 45 p. 8641 - 8647
反应条件
sodium hydrogencarbonate; L-proline in water
T=100°C; Wittig reaction; air; stereoselective reaction;
参考文献
McNulty, James; McLeod, David
Chemistry - A European Journal, 2011 , vol. 17, # 32 p. 8794 - 8798
反应条件
in dichloromethane
T=20 - 27°C; Wittig reaction;
参考文献
Orita, Akihiro; Okano, Junji; Uehara, Genta; Jiang, Lasheng; Otera, Junzo
Bulletin of the Chemical Society of Japan, 2007 , vol. 80, # 8 p. 1617 - 1623
