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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
243971-02-0
合成路线
（共 20 条）
1037493-30-3
→
反应条件
243971-02-0
反应条件
zinc dibromide in toluene T=130°C; 24 h;
参考文献
Cano, Rafael; Yus, Miguel; Ramon, Diego J.
Tetrahedron, 2012 , vol. 68, # 5 p. 1393 - 1400
120-72-9
吲哚
+
128796-39-4
4-三氟甲基苯硼酸
→
反应条件
243971-02-0
反应条件
oxygen; acetic acid; palladium diacetate T=20°C; P=760.051 Torr; 22 h;
参考文献
Yang, Shang-Dong; Sun, Chang-Liang; Fang, Zhao; Li, Bi-Jie; Li, Yi-Zhou; Shi, Zhang-Jie
Angewandte Chemie - International Edition, 2008 , vol. 47, # 8 p. 1473 - 1476
120-72-9
吲哚
+
455-13-0
4-碘三氟甲苯
→
反应条件
243971-02-0
反应条件
mono(bis(di-tert-butyl(4-(dimethylamino)phenyl)phosphonio)palladium(II))dichloride; 3,4,5,6-Tetrachlorophthalic anhydride; sodium hydroxide in ethanol; water T=80°C; 24 h; regioselective reaction;
参考文献
Lu, Guo-Ping; Cai, Chun
Synlett, 2012 , vol. 23, # 20 p. 2992 - 2996
1054567-14-4
→
反应条件
243971-02-0
反应条件
rhodium(II) heptafluorobutyrate in toluene T=60°C; 16 h; Molecular sieve;
参考文献
Shen, Meihua; Leslie, Brooke E.; Driver, Tom G.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 27 p. 5056 - 5059
128796-39-4
4-三氟甲基苯硼酸
+
167558-54-5
→
反应条件
243971-02-0
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate; potassium phosphate in toluene T=90°C; Suzuki-Miyaura coupling; 7 h;
参考文献
Fang, Yuan-Qing; Lautens, Mark
Journal of Organic Chemistry, 2008 , vol. 73, # 2 p. 538 - 549
945523-43-3
→
反应条件
1194058-37-1
+
243971-02-0
反应条件
5 Au/Fe2O3; hydrogen in toluene T=60 - 120°C; P=750.075 - 15001.5 Torr; 2 h; Autoclave; chemoselective reaction;
参考文献
Yamane, Yoshihiro; Liu, Xiaohao; Hamasaki, Akiyuki; Ishida, Tamao; Haruta, Masatake; Yokoyama, Takushi; Tokunaga, Makoto
Organic Letters, 2009 , vol. 11, # 22 p. 5162 - 5165
4248-19-5
氨基甲酸叔丁酯
+
370-99-0
→
反应条件
243971-02-0
反应条件
1: With copper(l) iodide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in toluene T=105°C; 24 h; Inert atmosphere; 2: With trifluoroacetic acid in dichloromethane T=23°C; 2 h; Inert atmosphere;
参考文献
Ackermann, Lutz; Barfuesser, Sebastian; Potukuchi, Harish K.
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 7-8 p. 1064 - 1072
1181455-16-2
→
反应条件
595548-60-0
+
1181455-67-3
+
243971-02-0
反应条件
1: With bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I) in benzene T=25°C; 16 h; Inert atmosphere; 2: With silica gel
参考文献
Organic Letters, , vol. 11, # 16 p. 3598 - 3601
1224876-17-8
→
反应条件
243971-02-0
反应条件
potassium tert-butylate; palladium diacetate; triphenylphosphine in dimethyl sulfoxide T=20 - 120°C; intramolecular Heck reaction; Inert atmosphere;
参考文献
Mao, Hui; Wan, Jie-Ping; Pan, Yuanjiang; Sun, Cuirong
Tetrahedron Letters, 2010 , vol. 51, # 14 p. 1844 - 1846
120-72-9
吲哚
+
402-43-7
对溴三氟甲苯
→
反应条件
1038826-06-0
+
243971-02-0
反应条件
lithium hydroxide hydrate; palladium diacetate; bis(1,1-diphenylphosphino)methane in water T=110°C; 18 h; regioselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 352, # 17 p. 2929 - 2936
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