反应条件
1.1: 87 percent / lithium bis(trimethylsilyl)amide / tetrahydrofuran / 0 - 45 °C
2.1: 94 percent / hydroxylamine hydrochloride; NaOH / methanol; H2O / Heating
3.1: frifluoroacetic anhydride; triethylamine / 1,2-dimethoxy-ethane / 0 - 20 °C
3.2: 44 percent / iron(II) chloride / 1,2-dimethoxy-ethane / 8 h / Heating
View Scheme
参考文献
Gudmundsson, Kristjan S.; Johns, Brian A.; Wang, Zhicheng; Turner, Elizabeth M.; Allen, Scott H.; Freeman, George A.; Boyd Jr., F. Leslie; Sexton, Connie J.; Selleseth, Dean W.; Moniri, Kelly R.; Creech, Katrina L.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 18 p. 5346 - 5361
