4-苄氧基-3-甲氧基苯硼酸合成路线 （共 3 条）
反应条件
1.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C 1.2: tetrahydrofuran / 2 h / -78 °C 2.1: HCl; water / diethyl ether View Scheme
参考文献
Synthetic Communications, , vol. 29, # 15 p. 2719 - 2730
反应条件
1.1: potassium carbonate / acetone / 24 h / |Inert atmosphere; |Reflux 2.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / |Inert atmosphere 2.2: 5 h / -78 - 20 °C / |Inert atmosphere 3.1: hydrogenchloride / water; tetrahydrofuran / -20 °C / pH 2 - 3 / |Inert atmosphere View Scheme
参考文献
Tetrahedron Letters, , vol. 54, # 38 p. 5178 - 5180
反应条件
1.1: potassium carbonate / acetone / 24 h / |Inert atmosphere; |Reflux 2.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / |Inert atmosphere 2.2: 5 h / -78 - 20 °C / |Inert atmosphere 3.1: hydrogenchloride / water; tetrahydrofuran / -20 °C / pH 2 - 3 / |Inert atmosphere View Scheme
参考文献
Tetrahedron Letters, , vol. 54, # 38 p. 5178 - 5180
