9H-吡啶并[2,3-b]吲哚合成路线 （共 33 条）
反应条件
1: 90 percent / t-BuONa; 1,1'-bis(diphenylphosphino)ferrocine / Pd2(dba)3 / toluene / 17 h / 100 °C 2: 31 percent / Na2CO3 / Pd(OAc)2 / dimethylformamide / 67 h / Heating View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 11 p. 1505 - 1510
反应条件
1.1: n-BuLi; TMEDA / tetrahydrofuran / 2.25 h / -70 - -10 °C 1.2: 50 percent / 1,2-dibromoethane / tetrahydrofuran / 2.25 h / -70 - -10 °C 2.1: 95 percent / KOH / methanol / 4 h / Heating 3.1: 90 percent / t-BuONa; 1,1'-bis(diphenylphosphino)ferrocine / Pd2(dba)3 / toluene / 17 h / 100 °C 4.1: 31 percent / Na2CO3 / Pd(OAc)2 / dimethylformamide / 67 h / Heating View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 11 p. 1505 - 1510
反应条件
1: 95 percent / KOH / methanol / 4 h / Heating 2: 90 percent / t-BuONa; 1,1'-bis(diphenylphosphino)ferrocine / Pd2(dba)3 / toluene / 17 h / 100 °C 3: 31 percent / Na2CO3 / Pd(OAc)2 / dimethylformamide / 67 h / Heating View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 11 p. 1505 - 1510
反应条件
1: aqueous hydrochloric acid; sodium nitrite; sodium azide 2: decalin / 180 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 73, p. 2626,2629
反应条件
in 1,4-dioxane 15 h; Irradiation;
参考文献
Heterocycles, , vol. 15, # 1 p. 483 - 487
反应条件
1: 5 percent / 0.17 h / 180 °C / microwave irradiation 2: 34 percent / H4P2O7 / 0.01 h / 170 °C / microwave irradiation View Scheme
参考文献
Organic Letters, , vol. 8, # 3 p. 415 - 418
反应条件
pyridine hydrochloride 0.25 h;
参考文献
Tetrahedron, , vol. 49, # 1 p. 49 - 64
反应条件
chloroform T=550 - 555°C; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 24 p. 3581 - 3585
参考文献
Journal of the American Chemical Society, , vol. 73, p. 2626,2629
反应条件
in water T=95°C; P=750.06 - 450036 Torr; various pressure; ΔV*; Rate constantProduct distribution;
参考文献
Journal of Physical Organic Chemistry, , vol. 9, # 9 p. 639 - 644
