sulfuryl dichloride in tetrachloromethane 2 h; Heating;

thionyl chloride effect of solvent, reaction time, irradiation and reagent on product/yield distribution; Product distribution;

in benzene-d6; benzene byproducts: (C6H5)3PO; (Ar or N2); addn. of silicon compd. to platinum complex, addn. of C6H6 and C6D6, keeping for several hours; sepn. of ppt., addn. of hexane to the mother liquor, drying ppt. in vac.for 2 h; elem. anal.;

in benzene-d6; benzene byproducts: (C6H5)3PO; (Ar or N2); addn. of silicon compd. to platinum complex, addn. of C6H6 and C6D6, keeping for several hours; sepn. of ppt., addn. of hexane to the mother liquor, drying ppt. in vac.for 2 h; elem. anal.;