1.1: t-BuOK / tetrahydrofuran / 0.25 h / 20 °C
1.2: 3.4 g / tetrahydrofuran / 0.5 h / 20 °C
2.1: 90 percent / PPTS / 5 h / Heating
3.1: 84 percent / PPTS / acetone; H2O / 96 h / 20 °C
4.1: 60 percent / NaHPO4; amylene; NaClO2 / acetone; H2O / 12 h / 20 °C
View Scheme
参考文献
Marion, Frederic; Williams, David E.; Patrick, Brian O.; Hollander, Irwin; Mallon, Robert; Kim, Steven C.; Roll, Deborah M.; Feldberg, Larry; Van Soest, Rob; Andersen, Raymond J.
Organic Letters, 2006 , vol. 8, # 2 p. 321 - 324
1: 90 percent / PPTS / 5 h / Heating
2: 84 percent / PPTS / acetone; H2O / 96 h / 20 °C
3: 60 percent / NaHPO4; amylene; NaClO2 / acetone; H2O / 12 h / 20 °C
View Scheme
参考文献
Marion, Frederic; Williams, David E.; Patrick, Brian O.; Hollander, Irwin; Mallon, Robert; Kim, Steven C.; Roll, Deborah M.; Feldberg, Larry; Van Soest, Rob; Andersen, Raymond J.
Organic Letters, 2006 , vol. 8, # 2 p. 321 - 324
1: 84 percent / PPTS / acetone; H2O / 96 h / 20 °C
2: 60 percent / NaHPO4; amylene; NaClO2 / acetone; H2O / 12 h / 20 °C
View Scheme
参考文献
Marion, Frederic; Williams, David E.; Patrick, Brian O.; Hollander, Irwin; Mallon, Robert; Kim, Steven C.; Roll, Deborah M.; Feldberg, Larry; Van Soest, Rob; Andersen, Raymond J.
Organic Letters, 2006 , vol. 8, # 2 p. 321 - 324
