反应条件
1: 94 percent / TBAF / tetrahydrofuran / 12 h / Ambient temperature 2: 1.) (COCl)2, DMSO, 2.) Et3N / 1.) CH2Cl2, -78 deg C, 45 min, 2.) -78 deg C to r.t., 12 h 3: SmI2 / tetrahydrofuran; methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Laine, Dramane; Fujita, Morifumi; Ley, Steven V.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 12 p. 1639 - 1645
