N,P-二(1,1-二甲基乙基)-氨基亚膦酰氯合成路线 (共 2 条)
参考文献
Harger, Martin J. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2127 - 2131
反应条件
in tetrahydrofuran
byproducts: LiCl, ((tBu)HNP(tBu))2; all manipulations in inert atm.; Pb and P compds. mixed in THF at -50°C, warmed to room temp.; volatiles removed;
参考文献
Herberhold, Max; Koehler, Christian; Troebs, Volker; Wrackmeyer, Bernd
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2000 , vol. 55, # 10 p. 939 - 945