四氟硼酸(1-甲基-3-辛基咪唑翁)合成路线 （共 9 条）
反应条件
potassium tetrafluoroborate T=120 - 140°C; 0.5 h; microwave irradiation; sonication;
参考文献
Cravotto, Giancarlo; Gaudino, Emanuela Calcio; Boffa, Luisa; Leveque, Jean-Marc; Estager, Julien; Bonrath, Werner
Molecules, 2008 , vol. 13, # 1 p. 149 - 156
反应条件
1: 0.25 h; 2: With sodium tetrafluoroborate in water
参考文献
Solvent Innovation GmbH
Patent: EP1182196 A1, 2002 ;
Location in patent: Page 12, 13 ;
反应条件
sodium tetrafluoroborate in dichloromethane T=70°C; 24 h; Inert atmosphereSchlenk techniqueGlovebox;
参考文献
Srour, Hassan; Rouault, Helene; Santini, Catherine C.; Chauvin, Yves
Green Chemistry, 2013 , vol. 15, # 5 p. 1341 - 1347
反应条件
potassium tetrafluoroborate T=140°C; 0.333333 h; microwave irradiation; sonication;
参考文献
Cravotto, Giancarlo; Boffa, Luisa; L'Eveque, Jean-Marc; Estager, Julien; Draye, Micheline; Bonrath, Werner
Australian Journal of Chemistry, 2007 , vol. 60, # 12 p. 946 - 950
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in acetonitrile T=20°C; Mitsunobu reaction;
参考文献
Petit, Sylvain; Azzouz, Rabah; Fruit, Corinne; Bischoff, Laurent; Marsais, Francis
Tetrahedron Letters, 2008 , vol. 49, # 22 p. 3663 - 3665
反应条件
1: NaBF4 / H2O View Scheme
参考文献
Journal of Solution Chemistry, , vol. 34, # 10 p. 1135 - 1144
反应条件
1: 48 h / Heating 2: aq. BF4H / 20 °C View Scheme
参考文献
Synthesis, , # 15 p. 2543 - 2550
反应条件
1: 2: With sodium tetrafluoroborate
参考文献
Organic Process Research and Development, , vol. 14, # 5 p. 1102 - 1109
参考文献
Journal of Chemical and Engineering Data, , vol. 59, # 3 p. 540 - 553
