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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-溴苯基硼酸
合成路线
（共 76 条）
99134-25-5
+
244205-40-1
2-溴苯基硼酸
→
反应条件
27973-36-0
9-亚芴基乙酸乙酯
反应条件
palladium diacetate; caesium carbonate; triphenylphosphine in N,N-dimethyl-formamide T=70°C; domino Suzuki/Heck coupling reaction; 1.5 h; Inert atmosphere;
参考文献
Paul, Sunanda; Gorai, Tumpa; Koley, Arijit; Ray, Jayanta K.
Tetrahedron Letters, 2011 , vol. 52, # 31 p. 4051 - 4055
719-98-2
+
244205-40-1
2-溴苯基硼酸
→
反应条件
1644-72-0
2-[(三氟甲基)硫代]溴苯
反应条件
[2,2']bipyridinyl; potassium carbonate; copper(l) chloride in ethylene glycol dimethyl ether T=45°C; 18 h; Schlenk techniqueInert atmosphereSealed tube;
参考文献
Pluta, Roman; Nikolaienko, Pavlo; Rueping, Magnus
Angewandte Chemie - International Edition, 2014 , vol. 53, # 6 p. 1650 - 1653
Angew. Chem., 2014 , vol. 126, # 6 p. 1676 - 1679,4
13194-69-9
2-碘-5-甲基苯胺
+
244205-40-1
2-溴苯基硼酸
→
反应条件
3652-91-3
2-甲基咔唑
反应条件
1: With caesium carbonate; tris(dibenzylideneacetone)dipalladium (0) in toluene 2: With sodium t-butanolate in toluene Further stages.;
参考文献
Kitamura, Yuki; Yoshikawa, Seiji; Furuta, Takumi; Kan, Toshiyuki
Synlett, 2008 , # 3 p. 377 - 380
244205-40-1
2-溴苯基硼酸
→
反应条件
3652-89-9
4-溴-9H-咔唑
反应条件
1: palladium diacetate; potassium carbonate; triphenylphosphine / ethanol; water; toluene / 18 h / 100 °C / Inert atmosphere 2: triphenylphosphine / N,N-dimethyl acetamide / 14 h / 180 °C / Inert atmosphere View Scheme
参考文献
Kim, Mounggon; Lee, Jun Yeob
Organic Electronics: physics, materials, applications, 2013 , vol. 14, # 1 p. 67 - 73
244205-40-1
2-溴苯基硼酸
+
191348-14-8
→
反应条件
18992-85-3
反应条件
1: With caesium carbonate; tris(dibenzylideneacetone)dipalladium (0) in toluene 2: With sodium t-butanolate in toluene Further stages.;
参考文献
Kitamura, Yuki; Yoshikawa, Seiji; Furuta, Takumi; Kan, Toshiyuki
Synlett, 2008 , # 3 p. 377 - 380
244205-40-1
2-溴苯基硼酸
→
反应条件
2005-10-9
反应条件
1: palladium diacetate; triphenylphosphine; sodium acetate / N,N-dimethyl-formamide / 3 h / 80 °C 2: pyridinium chlorochromate / dichloromethane / 20 °C View Scheme
参考文献
Wang, Yang; Gulevich, Anton V.; Gevorgyan, Vladimir
Chemistry - A European Journal, 2013 , vol. 19, # 47 p. 15836 - 15840
244205-40-1
2-溴苯基硼酸
→
反应条件
2005-10-9
+
69200-16-4
反应条件
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene; ethanol / |Reflux 2: 2-benzoyl-cyclohexanone; caesium carbonate; copper(I) thiophene-2-carboxylate / water / 0.17 h / 300 °C / 12929 Torr / |Microwave irradiation View Scheme
参考文献
Nealmongkol, Prattya; Tangdenpaisal, Kassrin; Sitthimonchai, Somkid; Ruchirawat, Somsak; Thasana, Nopporn
Tetrahedron, 2013 , vol. 69, # 44 p. 9277 - 9283
523-27-3
+
244205-40-1
2-溴苯基硼酸
→
反应条件
120-12-7
+
197-61-5
+
203-33-8
+
192-42-7
反应条件
tris(dibenzylideneacetone)dipalladium (0); 1,8-diazabicyclo[5.4.0]undec-7-ene; tri-cyclo-hexyl-phosphine in N,N-dimethyl-formamide T=155°C; Suzuki coupling, Heck coupling; 48 h;
参考文献
Wegner, Hermann A.; Scott, Lawrence T.; De Meijere, Armin
Journal of Organic Chemistry, 2003 , vol. 68, # 3 p. 883 - 887
109-04-6
+
244205-40-1
2-溴苯基硼酸
→
反应条件
109306-86-7
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethanol; water; toluene Suzuki coupling; 24 h; Inert atmosphereReflux;
参考文献
Rao, Ying-Li; Amarne, Hazem; Zhao, Shu-Bin; McCormick, Theresa M.; Martic, Sanela; et al.
Journal of the American Chemical Society, 2008 , vol. 130, p. 12898 - 12900
824-54-4
+
244205-40-1
2-溴苯基硼酸
→
反应条件
1705-89-1
反应条件
sodium acetate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=120°C; Suzuki coupling; 15 h; Inert atmosphere;
参考文献
Paul, Sunanda; Samanta, Shubhankar; Ray, Jayanta K.
Tetrahedron Letters, 2010 , vol. 51, # 42 p. 5604 - 5608
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