(7CI,8CI)-m-(对甲苯)-苯甲醚合成路线 （共 44 条）
反应条件
lithium tert-butylate; [NiCl2(PMe3)2] in tetrahydrofuran
T=60°C; 2 h;
参考文献
Miller, Joseph A.
Tetrahedron Letters, 2001 , vol. 42, # 40 p. 6991 - 6993
反应条件
N-hexadecyl-N,N,N-trimethylammonium bromide; sodium hydroxide in water
T=25°C; Suzuki Coupling; 1 h; Microwave irradiation; Catalytic behavior;
参考文献
Wang, Feng; Li, Chuanhao; Chen, Huanjun; Jiang, Ruibin; Sun, Ling-Dong; Li, Quan; Wang, Jianfang; Yu, Jimmy C.; Yan, Chun-Hua
Journal of the American Chemical Society, 2013 , vol. 135, # 15 p. 5588 - 5601
反应条件
tetrabutyl ammonium fluoride; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tetrahydrofuran; tert-butyl alcohol
T=90°C; Hiyama coupling; Inert atmosphere;
参考文献
Zhang, Liang; Qing, Jiang; Yang, Pengyuan; Wu, Jie
Organic Letters, 2008 , vol. 10, # 21 p. 4971 - 4974
反应条件
3,3'-(3,4-bis(dichloromethylene)cyclobut-1-ene-1,2-diyl)bis(1-methyl-1H-imidazolium) bis(tetrafluoroborate); palladium diacetate; sodium t-butanolate in toluene
T=20°C; Suzuki-Miyaura coupling; 2 h; Inert atmosphere;
参考文献
Schmidt, Andreas; Rahimi, Alireza
Chemical Communications, 2010 , vol. 46, # 17 p. 2995 - 2997
反应条件
bis(1,5-cyclooctadiene)nickel (0); hydrogen; trimethylaluminum; tri-cyclo-hexyl-phosphine in toluene
T=130°C; P=750.075 Torr; 24 h; Schlenk technique;
参考文献
Patra, Tuhin; Agasti, Soumitra; Modak, Atanu; Maiti, Debabrata
Chemical Communications, 2013 , vol. 49, # 75 p. 8362 - 8364
反应条件
CuF2; Ni(PCy3)2Cl2; potassium tert-butylate; tri-cyclo-hexyl-phosphine in 1,4-dioxane
T=110°C; Suzuki-Miyaura coupling; 20 h; Inert atmosphere;
参考文献
Yu, Da-Gang; Yu, Miao; Guan, Bing-Tao; Li, Bi-Jie; Zheng, Yang; Wu, Zhen-Hua; Shi, Zhang-Jie
Organic Letters, 2009 , vol. 11, # 15 p. 3374 - 3377
反应条件
Ni(PCy3)2Cl2 in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=90°C; Negishi coupling reaction; 8 h; Inert atmosphere;
参考文献
Xie, Lan-Gui; Wang, Zhong-Xia
Angewandte Chemie - International Edition, 2011 , vol. 50, # 21 p. 4901 - 4904
反应条件
3,3'-(3,4-bis(dichloromethylene)cyclobut-1-ene-1,2-diyl)bis(1-methyl-1H-imidazolium) bis(tetrafluoroborate); palladium diacetate; sodium t-butanolate in toluene
T=50°C; Suzuki-Miyaura reaction; 3 h;
参考文献
Rahimi, Alireza; Papai, Imre; Madarasz, Udam; Gjikaj, Mimoza; Namyslo, Jan C.; Schmidt, Andreas
European Journal of Organic Chemistry, 2012 , # 4 p. 754 - 763
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in toluene
Suzuki-Miyaura reaction; 24 h; Heating;
参考文献
Cammidge, Andrew N.; Goddard, Victoria H. M.; Gopee, Hemant; Harrison, Nicola L.; Hughes, David L.; Schubert, Christopher J.; Sutton, Benjamin M.; Watts, Gary L.; Whitehead, Andrew J.
Organic Letters, 2006 , vol. 8, # 18 p. 4071 - 4074
反应条件
1: (4-methylphenyl)trichlorogermane With ammonium hydroxide
T=20°C; 1 h;
2: 3-methoxy-iodobenzene With sodium hydroxide; palladium diacetate in 1,4-dioxane; water
4 h; Heating; Further stages.;
参考文献
Endo, Mayuko; Fugami, Keigo; Enokido, Tatsuki; Sano, Hiroshi; Kosugi, Masanori
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 7 p. 1025 - 1027
