1,1-二碘-2,2-二甲基丙烷合成路线 (共 9 条)
反应条件
magnesium iodide in carbon disulfide T=0°C; 0.25 h;
参考文献
Garcia Martinez, A.; Herrera Fernandez, A.; Martinez Alvarez, R.; Garcia Fraile, A.; Bueno Calderon, J.; et al.
Synthesis, 1986 , # 12 p. 1076 - 1078
反应条件
pyridine; iodine cloride in dichloromethane T=-20°C;
参考文献
Fry,A.J.; Cawse,J.N.
Journal of Organic Chemistry, 1967 , vol. 32, p. 1677 - 1679
反应条件
(i) aq. N2H4, Et3N, EtOH, (ii) I2, Et3N, Et2O; Multistep reaction;
参考文献
Fry,A.J.; Cawse,J.N.
Journal of Organic Chemistry, 1967 , vol. 32, p. 1677 - 1679
反应条件
iodine; triethylamine in diethyl ether Ambient temperature;
参考文献
Pross,A.; Sternhell,S.
Australian Journal of Chemistry, 1970 , vol. 23, p. 989 - 1003
反应条件
in 1,2-dichloro-ethane; cyclohexene 20 h; Irradiation;
参考文献
Moret, Etienne; Jones, Carol R.; Grant, Barbara
Journal of Organic Chemistry, 1983 , vol. 48, # 12 p. 2090 - 2092
反应条件
T=146°C; heated tube packed with methyllithium-coated glass chips; Yield given. Yields of byproduct given;
参考文献
Fukushima, Motoo; Jones, Maitland; Brinker, Udo H.
Tetrahedron Letters, 1982 , vol. 23, # 32 p. 3211 - 3214
反应条件
in cyclohexene 4 h; Irradiation;
参考文献
Kropp, Paul J.; Pienta, Norbert J.
Journal of Organic Chemistry, 1983 , vol. 48, # 12 p. 2084 - 2090
反应条件
in 1,2-dichloro-ethane; cyclohexene 20 h; Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 48, # 12 p. 2084 - 2090
反应条件
T=146°C; heated tube packed with methyllithium-coated glass chips; Yield given. Yields of byproduct given;
参考文献
Fukushima, Motoo; Jones, Maitland; Brinker, Udo H.
Tetrahedron Letters, 1982 , vol. 23, # 32 p. 3211 - 3214