苯并[B]噻吩-3-甲醛合成路线 （共 27 条）
反应条件
in N,N-dimethyl acetamide 72 h; Heating;
参考文献
Dit Chabert, Jeremie Fournier; Joucla, Lionel; David, Emilie; Lemaire, Marc
Tetrahedron, 2004 , vol. 60, # 14 p. 3221 - 3230
参考文献
Journal of Scientific and Industrial Research, , vol. 15 B, p. 627
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 236, p. 385
反应条件
[BMIM(SO3H)][OTf]; trimethylsilylazide; 1-n-butyl-3-methylimidazolium hexafluorophosphate T=20 - 50°C; Schmidt Reaction; 3 h; Sonication;
参考文献
Nandi, Ganesh C.; Laali, Kenneth K.
Tetrahedron Letters, 2013 , vol. 54, # 17 p. 2177 - 2179
反应条件
in methanol 46 h; Ambient temperaturePt foil electrode, 0.1 A constant current;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 3 p. 333 - 336
反应条件
water in tetrahydrofuran; diethyl ether T=-80°C; 0.0833333 h; Product distribution;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 92, # 1 p. 53 - 60
反应条件
water in tetrahydrofuran; diethyl ether T=-80°C; 0.0833333 h; Product distribution;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 92, # 1 p. 53 - 60
参考文献
Mitra et al.
Journal of Scientific and Industrial Research, 1956 , vol. 15 B, p. 627
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; 1,2-bis-(diphenylphosphino)ethane in chlorobenzene 6 h; Inert atmosphereReflux;
参考文献
Arisawa, Mieko; Toriyama, Fumihiko; Yamaguchi, Masahiko
Tetrahedron Letters, 2011 , vol. 52, # 18 p. 2344 - 2347
反应条件
tetrabutylammomium bromide; potassium carbonate; palladium diacetate in N,N-dimethyl-formamide T=140°C; Heck-type reaction; 1.5 h;
参考文献
Fournier Dit Chabert, Jeremie; Gozzi, Christel; Lemaire, Marc
Tetrahedron Letters, 2002 , vol. 43, # 10 p. 1829 - 1833
反应条件
2,3,11,12-dicyclohexano-1,4,7,10,13,16-hexaoxacyclo-octadecane; palladium diacetate; potassium carbonate in dimethyl sulfoxide T=140°C; Heck reaction; 17 h;
参考文献
Dit Chabert, Jeremie Fournier; Joucla, Lionel; David, Emilie; Lemaire, Marc
Tetrahedron, 2004 , vol. 60, # 14 p. 3221 - 3230
