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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2446-51-7
合成路线
（共 67 条）
67-56-1
甲醇
+
951654-95-8
→
反应条件
反应条件
oxygen Photolysis; Product distribution; Further Variations:Reagentsirradiation wavelength;
参考文献
Desikan, Vasumathi; Liu, Yonglin; Toscano, John P.; Jenks, William S.
Journal of Organic Chemistry, 2007 , vol. 72, # 18 p. 6848 - 6859
67-56-1
甲醇
+
61820-48-2
→
反应条件
6086-21-1
1-甲基-1,2,4-三唑
+
2446-51-7
反应条件
Ambient temperatureIrradiationphotochemistry of other N-(benzoylimino)-1,2,4-triazolium and N-(benzoylomino)pyridinium ylides; Mechanism;
参考文献
Arnold, Charles R.; Melvin, Tracy; Nelson, William M.; Schuster, Gary B.
Journal of Organic Chemistry, 1992 , vol. 57, # 12 p. 3316 - 3319
201230-82-2
+
2446-51-7
→
反应条件
1914-20-1
N-甲氧基邻苯二甲酰亚胺
反应条件
1: carbon monoxide With acetic acid 0.166667 h; 2: PhC(O)NH(OMe) With palladium diacetate; p-benozquinone T=50 - 110°C; 18 h;
参考文献
Wrigglesworth, Joe W.; Cox, Brian; Lloyd-Jones, Guy C.; Booker-Milburn, Kevin I.
Organic Letters, 2011 , vol. 13, # 19 p. 5326 - 5329
292638-84-7
+
2446-51-7
→
反应条件
26278-74-0
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; sodium acetate in 2,2,2-trifluoroethanol T=50°C; 24 h; Inert atmosphere;
参考文献
Li, Bin; Ma, Jianfeng; Wang, Nuancheng; Feng, Huiliang; Xu, Shansheng; Wang, Baiquan
Organic Letters, 2012 , vol. 14, # 3 p. 736 - 739
2446-51-7
+
780-69-8
苯基三乙氧基硅烷
→
反应条件
69605-58-9
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; copper diacetate; silver fluoride in 1,2-dichloro-ethane T=60°C; 3 h; Inert atmosphereSealed tube; Reagent/catalystSolvent; regioselective reaction;
参考文献
Senthilkumar, Natarajan; Parthasarathy, Kanniyappan; Gandeepan, Parthasarathy; Cheng, Chien-Hong
Chemistry - An Asian Journal, 2013 , vol. 8, # 9 p. 2175 - 2181
2446-51-7
+
71-43-2
苯
→
反应条件
69605-58-9
反应条件
dipotassium peroxodisulfate; palladium diacetate; trifluoroacetic acid in toluene T=25°C; 16 h; Inert atmosphereSealed; regioselective reaction;
参考文献
Karthikeyan, Jaganathan; Cheng, Chien-Hong
Angewandte Chemie - International Edition, 2011 , vol. 50, # 42 p. 9880 - 9883
2446-51-7
+
98-80-6
苯硼酸
→
反应条件
69605-58-9
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; silver(l) oxide in methanol T=60°C; 3 h; Inert atmosphereSealed tubeSchlenk technique; SolventReagent/catalystTemperature;
参考文献
Karthikeyan, Jaganathan; Haridharan, Radhakrishnan; Cheng, Chien-Hong
Angewandte Chemie - International Edition, 2012 , vol. 51, # 49 p. 12343 - 12347
Angew. Chem., 2012 , vol. 124, # 49 p. 12509 - 12513,4
591-50-4
碘苯
+
2446-51-7
→
反应条件
69605-58-9
反应条件
palladium diacetate; acetic acid; silver(l) oxide T=120°C; 36 h;
参考文献
Wang, Guan-Wu; Yuan, Ting-Ting; Li, Dan-Dan
Angewandte Chemie - International Edition, 2011 , vol. 50, # 6 p. 1380 - 1383
2446-51-7
+
1268451-51-9
+
98-80-6
苯硼酸
→
反应条件
69605-58-9
+
1435477-75-0
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; silver(l) oxide in methanol; dichloromethane T=60°C; 0.5 h; Inert atmosphereSealed tube;
参考文献
Karthikeyan, Jaganathan; Haridharan, Radhakrishnan; Cheng, Chien-Hong
Angewandte Chemie - International Edition, 2012 , vol. 51, # 49 p. 12343 - 12347
Angew. Chem., 2012 , vol. 124, # 49 p. 12509 - 12513,4
2446-51-7
+
10365-98-7
3-甲氧基苯硼酸
+
98-80-6
苯硼酸
→
反应条件
69605-58-9
+
1275595-52-2
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; silver(l) oxide in methanol; dichloromethane T=60°C; 0.5 h; Inert atmosphereSealed tube;
参考文献
Karthikeyan, Jaganathan; Haridharan, Radhakrishnan; Cheng, Chien-Hong
Angewandte Chemie - International Edition, 2012 , vol. 51, # 49 p. 12343 - 12347
Angew. Chem., 2012 , vol. 124, # 49 p. 12509 - 12513,4
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