2-甲基-2-丙基(2E)-2-亚苄基肼羧酸酯合成路线 (共 5 条)
反应条件
1: BH3*THF / tetrahydrofuran / 0.17 h / Ambient temperature 2: 6 N aq. HCl / tetrahydrofuran / 0.17 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 46, # 26 p. 5413 - 5414
反应条件
1: H2 / 10percent Pd/C
2: Al2O3
View Scheme
参考文献
Sham, Hing L.; Betebenner, David A.; Zhao, Chen; Wideburg, Norman E.; Saldivar, Ayda; et al.
Journal of the Chemical Society, Chemical Communications, 1993 , # 13 p. 1052 - 1053
反应条件
1: H2 / Pd-C / tetrahydrofuran
2: aq. NaOH / CHCl3
3: aq. HCl / ethyl acetate
View Scheme
参考文献
Dutta; Morley
Journal of the Chemical Society. Perkin transactions 1, 1975 , # 17 p. 1712 - 1720
反应条件
1: 27 percent / ammonium formate / Pd/C / methanol / 2 h
2: 54 percent / Et3N / ethyl acetate / 0 °C
View Scheme
参考文献
Dutta; Morley
Journal of the Chemical Society. Perkin transactions 1, 1975 , # 17 p. 1712 - 1720
反应条件
hydrogen; palladium on activated charcoal in methanol
P=1551.44 Torr; 0.333333 h;
参考文献
Melendez, Rosa E.; Lubell, William D.
Journal of the American Chemical Society, 2004 , vol. 126, # 21 p. 6759 - 6764