反应条件
1.1: potassium bis(trimethylsilyl)amide / tetrahydrofuran; toluene / 1 h / -78 °C
1.2: 99 percent / tetrahydrofuran; toluene / 0.33 h / -23 °C
2.1: tributylamine; bis(acetato)bis(triphenylphosphine)palladium(II); formic acid / dimethylformamide / 7 h / 60 °C
3.1: 14 mg / tetra-n-butylammonium fluoride / tetrahydrofuran / 2 h / 20 °C
View Scheme
参考文献
Nakamura, Tsuyoshi; Shiozaki, Masao
Tetrahedron Letters, 1999 , vol. 40, # 51 p. 9063 - 9064