2-甲基-3-甲氧基苯甲酰氯合成路线 （共 13 条）
反应条件
thionyl chloride in xylene T=20 - 135°C; 3 h;
参考文献
Scherer, Johannes; Mueller-Hauck, Friedrich
Patent: US2004/260119 A1, 2004 ;
Location in patent: Page 6 ;
反应条件
thionyl chloride in chloroform
反应条件
1: 60 percent / 5N HCl / 12 h / Heating 2: thionyl chloride, DMF / CHCl3 / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 32, # 2 p. 409 - 417
反应条件
1: 89 percent / n-BuLi 2: 60 percent / 5N HCl / 12 h / Heating 3: thionyl chloride, DMF / CHCl3 / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 32, # 2 p. 409 - 417
反应条件
1: aqueous alkaline solution / anschliessend Hydrolyse 2: thionyl chloride View Scheme
参考文献
Journal of the American Chemical Society, , vol. 58, p. 749,753
反应条件
1: aq. NaOH solution / 250 - 275 °C 2: aqueous alkaline solution / anschliessend Hydrolyse 3: thionyl chloride View Scheme
参考文献
Journal of the American Chemical Society, , vol. 58, p. 749,753
参考文献
Fieser; Lothrop
Journal of the American Chemical Society, 1936 , vol. 58, p. 749,753
反应条件
triethylamine Acylation; 4 h;
参考文献
Nakagawa, Yoshiaki; Hattori, Kazunari; Minakuchi, Chieka; Kugimiya, Soichi; Ueno, Tamio
Steroids, 2000 , vol. 65, # 3 p. 117 - 123
反应条件
potassium carbonate; hydrazine in dichloromethane; water
T=0 - 20°C; 2.5 h;
参考文献
Hormann, Robert Eugene; Chortyk, Orestes; Le, Dat Phat
Patent: US2004/171651 A1, 2004 ;
Location in patent: Page/Page column 37 ;
Title/Abstract Full Text Show Details
Chortyk, Orestes; Le, Dat Phat; Hormann, Robert Eugene
Patent: US2004/171651 A1, 2004 ;
Location in patent: Page/Page column 37 ;
反应条件
potassium carbonate; hydrazine in dichloromethane; water
T=0 - 10°C; 1.5 - 2 h;
参考文献
Hormann, Robert Eugene; Tice, Colin M.; Chortyk, Orestes; Smith, Howard; Meteyer, Thomas
Patent: US2005/209283 A1, 2005 ;
Location in patent: Page/Page column 26 ;
