3-硝基-2,4-吡啶二胺合成路线 （共 10 条）
反应条件
ammonia in water T=91°C; P=3067.81 Torr; 7 h; Industrial scale;
参考文献
Cleator, Ed; Scott, Jeremy P.; Avalle, Paulo; Bio, Matthew M.; Brewer, Sarah E.; Davies, Antony J.; Gibb, Andrew D.; Sheen, Faye J.; Stewart, Gavin W.; Wallace, Debra J.; Wilson., Robert D.
Organic Process Research and Development, 2013 , vol. 17, # 12 p. 1561 - 1567
反应条件
1: nitric acid 2: phosphoryl chloride 3: ethanolic NH3 / 100 °C View Scheme
参考文献
Cleator, Ed; Scott, Jeremy P.; Avalle, Paulo; Bio, Matthew M.; Brewer, Sarah E.; Davies, Antony J.; Gibb, Andrew D.; Sheen, Faye J.; Stewart, Gavin W.; Wallace, Debra J.; Wilson., Robert D.
Organic Process Research and Development, 2013 , vol. 17, # 12 p. 1561 - 1567
反应条件
1: phosphoryl chloride 2: ethanolic NH3 / 100 °C View Scheme
参考文献
Cleator, Ed; Scott, Jeremy P.; Avalle, Paulo; Bio, Matthew M.; Brewer, Sarah E.; Davies, Antony J.; Gibb, Andrew D.; Sheen, Faye J.; Stewart, Gavin W.; Wallace, Debra J.; Wilson., Robert D.
Organic Process Research and Development, 2013 , vol. 17, # 12 p. 1561 - 1567
参考文献
Talik; Plazek
Roczniki Chemii, 1956 , vol. 30, p. 1139,1145
Chem.Abstr., <1957> 12089
反应条件
1.1: trichlorophosphate; lithium chloride / 2.5 h / 105 °C / |Industrial scale 1.2: 1 h / 105 °C / |Industrial scale 2.1: ammonia / water / 7 h / 91 °C / 3067.81 Torr / |Industrial scale View Scheme
参考文献
Cleator, Ed; Scott, Jeremy P.; Avalle, Paulo; Bio, Matthew M.; Brewer, Sarah E.; Davies, Antony J.; Gibb, Andrew D.; Sheen, Faye J.; Stewart, Gavin W.; Wallace, Debra J.; Wilson., Robert D.
Organic Process Research and Development, 2013 , vol. 17, # 12 p. 1561 - 1567
反应条件
1: KNO3; aqueous HNO3 2: water / 140 °C 3: phosphoryl chloride 4: ethanolic NH3 / 100 °C View Scheme
参考文献
Koegl et al.
Recueil des Travaux Chimiques des Pays-Bas, 1948 , vol. 67, p. 29,37
反应条件
1: acetic acid; concentrated aqueous HNO3 2: aqueous NaOH 3: water / 140 °C 4: phosphoryl chloride 5: ethanolic NH3 / 100 °C View Scheme
参考文献
Koegl et al.
Recueil des Travaux Chimiques des Pays-Bas, 1948 , vol. 67, p. 29,37
反应条件
1: water / 140 °C 2: phosphoryl chloride 3: ethanolic NH3 / 100 °C View Scheme
参考文献
Koegl et al.
Recueil des Travaux Chimiques des Pays-Bas, 1948 , vol. 67, p. 29,37
反应条件
1: aqueous NaOH 2: water / 140 °C 3: phosphoryl chloride 4: ethanolic NH3 / 100 °C View Scheme
参考文献
Koegl et al.
Recueil des Travaux Chimiques des Pays-Bas, 1948 , vol. 67, p. 29,37
反应条件
ethanol; nickel Hydrogenation;
参考文献
Koegl et al.
Recueil des Travaux Chimiques des Pays-Bas, 1948 , vol. 67, p. 29,37
