1,1-二甲基-2-丙烯基乙酸酯合成路线 （共 69 条）
反应条件
NiCl2TPP; isopropylmagnesium chloride in tetrahydrofuran
T=20°C; 36 h; var. ligands, temp., times; Product distribution;
参考文献
Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. C21 - C24
反应条件
methylmagnesium bromide; sodium hydride; NiCl2((PPh3)P)2 in tetrahydrofuran
T=65°C; 36 h; other reag.; other catalyst; other temp./react. time; other solvents; Product distribution;
参考文献
Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1986 , vol. 317, p. 383 - 408
反应条件
NiCl2TPP; isopropylmagnesium chloride in tetrahydrofuran
T=20°C; 36 h; var. ligands, temp., times; Product distribution;
参考文献
Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. C21 - C24
反应条件
sodium hydride; bis-diphenylphosphinoethane; Pd(1,2-bis(diphenylphosphino)ethane)2 in tetrahydrofuran
36 h; Heating;
参考文献
Cuvigny, Therese; Julia, Marc; Rolando, C.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 395 - 414
反应条件
silver hexafluoroantimonate; 1,10-phenanthroline; palladium diacetate in 1,2-dichloro-ethane
T=60°C; 12 h; Inert atmosphere; regiospecific reaction;
参考文献
Ohmiya, Hirohisa; Makida, Yusuke; Tanaka, Tatsunori; Sawamura, Masaya
Journal of the American Chemical Society, 2008 , vol. 130, # 51 p. 17276 - 17277
反应条件
lithium chloride; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide
T=23°C; 27 h;
参考文献
Valle, L. Del; Stille, J. K.; Hegedus, L. S.
Journal of Organic Chemistry, 1990 , vol. 55, p. 3019 - 3023
参考文献
Nesmejanow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1951 , p. 273,277
Chem.Abstr., 1952 , p. 882
反应条件
lt;Mo(CO)4Br2gt;2 in dichloromethane
1.5 h; Ambient temperature; Yield givenYields of byproduct given;
参考文献
Malkov, Andrei V.; Davis, Stuart L.; Baxendale, Ian R.; Mitchell, William L.; Kocovsky, Pavel
Journal of Organic Chemistry, 1999 , vol. 64, # 8 p. 2751 - 2764
反应条件
isopropylmagnesium chloride; sodium hydride; NiCl2((CH2)4(PPh3)2)2 in tetrahydrofuran
T=45°C; 24 h; other catalyst; other temp./react. time; other solvent; Product distribution;
参考文献
Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1986 , vol. 317, p. 383 - 408
反应条件
tetrakis(triphenylphosphine) palladium(0); 18-crown-6 ether; carbon dioxide; potassium carbonate
T=75°C; Tsuji-Trost Allylation; P=129209 Torr; 18 h; Supercritical conditionsAutoclave; Overall yield = 25 percent;
参考文献
Vasil'ev, Andrei A.; Kuchurov, Ilya V.; Zlotin, Sergei G.
Mendeleev Communications, 2013 , vol. 23, # 2 p. 84 - 85
