5-氯吡唑并[1,5-a]嘧啶-7-胺合成路线 (共 2 条)
反应条件
ammonium hydroxide T=20 - 85°C; Sealed tube;
参考文献
SCHERING CORPORATION; MENG, Zhaoyang; REDDY, Panduranga Adulla, P.; SIDDIQUI, M. Arshad; MANDAL, Amit, K.; LIU, Duan; ZHAO, Lianyun; MCRINER, Andrew
Patent: WO2012/27234 A1, 2012 ;
Location in patent: Page/Page column 40 ;
WO 2012/027234 A1
反应条件
1: trichlorophosphate; N,N-dimethyl-aniline / 16 h / 0 - 60 °C / Inert atmosphere 2: ammonium hydroxide / 20 - 85 °C / Sealed tube View Scheme
参考文献
SCHERING CORPORATION; MENG, Zhaoyang; REDDY, Panduranga Adulla P.; SIDDIQUI, M. Arshad
Patent: WO2012/47569 A1, 2012 ;
WO 2012/047569 A1