(1R,2R)-2-((叔丁氧基羰基)氨基)环戊烷羧酸乙酯合成路线 （共 3 条）
反应条件
1: HN3; Ph3P; diethyl azodicarboxylate / benzene; ethanol / 8 h / 10 - 20 °C 2: Ph3P; H2O / tetrahydrofuran / 18 h 3: 18 percent / tetrahydrofuran / 48 h View Scheme
参考文献
Appella, Daniel H.; Christianson, Laurie A.; Klein, Daniel A.; Richards, Michele R.; Powell, Douglas R.; Gellman, Samuel H.
Journal of the American Chemical Society, 1999 , vol. 121, # 33 p. 7574 - 7581
反应条件
in tetrahydrofuran Acylation; 48 h;
参考文献
Appella, Daniel H.; Christianson, Laurie A.; Klein, Daniel A.; Richards, Michele R.; Powell, Douglas R.; Gellman, Samuel H.
Journal of the American Chemical Society, 1999 , vol. 121, # 33 p. 7574 - 7581
反应条件
lithium hydroxide; dihydrogen peroxide in methanol T=5°C; Hydrolysis; 20 h;
参考文献
Appella, Daniel H.; Christianson, Laurie A.; Klein, Daniel A.; Richards, Michele R.; Powell, Douglas R.; Gellman, Samuel H.
Journal of the American Chemical Society, 1999 , vol. 121, # 33 p. 7574 - 7581
