9-乙基-9H-咔唑-3-磺酰氯合成路线 （共 3 条）
反应条件
chlorosulfonic acid in tetrachloromethane T=5°C; 1 h;
参考文献
Zhang, Jun; Cui, Huiling; Hojo, Masashi; Shuang, Shaomin; Dong, Chuan
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 1 p. 343 - 346
反应条件
phosphorus pentachloride; trichlorophosphate T=90°C; 2 h;
参考文献
Hu, Laixing; Li, Zhuo-rong; Wang, Yue-ming; Wu, Yanbin; Jiang, Jian-Dong; Boykin, David W.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 5 p. 1193 - 1196
反应条件
1.1: potassium hydroxide / acetone / 0.5 h / 20 °C 1.2: 10 h / 20 °C 2.1: chlorosulfonic acid / tetrachloromethane / 1 h / 5 °C View Scheme
参考文献
Zhang, Jun; Cui, Huiling; Hojo, Masashi; Shuang, Shaomin; Dong, Chuan
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 1 p. 343 - 346
