1,3-二氧杂环己烷-2-酮合成路线 （共 26 条）
反应条件
air; potassium iodide; PdI2 in isobutyramide T=100°C; P=15201 Torr; 15 h; Autoclave;
参考文献
Tetrahedron Letters, , vol. 50, # 52 p. 7330 - 7332
反应条件
tri-cyclo-hexyl-phosphine in toluene T=110°C; P=26252.6 Torr; 24 h;
参考文献
Journal of the American Chemical Society, , vol. 130, # 20 p. 6523 - 6533
反应条件
caesium carbonate in N,N-dimethyl-formamide T=40°C; P=760.051 Torr; 15 h; Inert atmosphereGloveboxGreen chemistry; Reagent/catalystTemperature;
参考文献
Green Chemistry, , vol. 15, # 8 p. 2086 - 2090
反应条件
sodium hydroxide in chloroform T=61°C; 1.5 h; Inert atmosphere;
参考文献
US2010/123097 A1, ;
Page/Page column 8 ;
反应条件
bis(acetylacetonate)oxovanadium; tetrabutylammomium bromide in toluene T=60°C; P=26252.6 Torr; 8 h; AutoclaveCooling with ice; chemoselective reaction;
参考文献
Green Chemistry, , vol. 12, # 8 p. 1376 - 1379
反应条件
sodium methylate T=100 - 170°C;
参考文献
Canadian Journal of Chemistry, , vol. 82, # 12 p. 1769 - 1773
反应条件
tributyltin chloride in N,N-dimethyl-formamide T=60°C; 8 h;
参考文献
Chemistry Letters, , p. 749 - 752
反应条件
in 1,2-dichloro-ethane
反应条件
triethylamine in tetrahydrofuran
参考文献
Tetrahedron, , vol. 64, # 18 p. 4126 - 4134
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile T=20°C; cyclocondensation;
参考文献
Journal of Organic Chemistry, , vol. 65, # 20 p. 6368 - 6380
