1,3-二氧杂环己烷-2-酮合成路线 (共 26 条)
反应条件
1: With Novozym.(R).435 T=60°C; 7 h; Molecular sieveEnzymatic reaction; 2: T=90°C; 40 h; chemoselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 5 p. 797 - 802
反应条件
T=120°C; 1 h; Molecular sieve;
参考文献
WO2012/158107 A1, ;
Page/Page column 16 ;
反应条件
hydrogenchloride in acetonitrile-D3; water-d2
参考文献
Tetrahedron Letters, , vol. 35, # 31 p. 5641 - 5644
反应条件
hydrogenchloride in acetonitrile-D3; water-d2
参考文献
Tetrahedron Letters, , vol. 35, # 31 p. 5641 - 5644
反应条件
dibenzoyl peroxide T=100°C; 2 h; other temperature; Rate constantProduct distribution;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 53, # 10 p. 2363 - 2367,2131 - 2134
反应条件
dibenzoyl peroxide T=100°C; 2 h; other temperature; Rate constantProduct distribution;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 53, # 10 p. 2363 - 2367,2131 - 2134
反应条件
di-tert-butyl peroxide in chlorobenzene T=130°C; Product distributionRate constantMechanism;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, # 1 p. 127 - 132
Zhurnal Organicheskoi Khimii, , vol. 19, # 1 p. 139 - 144
反应条件
di-tert-butyl peroxide T=130°C; 0.5 h; Product distribution;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, # 1 p. 127 - 132
Zhurnal Organicheskoi Khimii, , vol. 19, # 1 p. 139 - 144
反应条件
Na-Y zeolite in triglyme (triethylene glycol dimethyl ether) 8 h; Heating;
参考文献
Shivarkar, Anandkumar B.; Gupte, Sunil P.; Chaudhari, Raghunath V.
Synlett, 2006 , # 9 p. 1374 - 1378