4-(3-(丙烯酰氧基)丙氧基)苯甲酸合成路线 （共 4 条）
反应条件
2,6-di-tert-butyl-4-methyl-phenol; triethylamine in tetrahydrofuran T=0 - 45°C;
参考文献
Martinelli, Elisa; Paoli, Francesca; Gallot, Bernard; Galli, Giancarlo
Journal of Polymer Science, Part A: Polymer Chemistry, 2010 , vol. 48, # 18 p. 4128 - 4139
反应条件
toluene-4-sulfonic acid; hydroquinone in tetrahydrofuran; hexane; toluene 8 h; Heating / reflux;
参考文献
DAINIPPON INK AND CHEMICALS, INC.
Patent: EP1174412 A1, 2002 ;
Location in patent: Page 76 ;
反应条件
1.1: potassium carbonate / butanone / 48 h / Reflux 2.1: water; potassium hydroxide / ethanol / 6 h / Reflux 2.2: pH 2 3.1: 2,6-di-tert-butyl-4-methyl-phenol; triethylamine / tetrahydrofuran / 0 - 45 °C View Scheme
参考文献
Martinelli, Elisa; Paoli, Francesca; Gallot, Bernard; Galli, Giancarlo
Journal of Polymer Science, Part A: Polymer Chemistry, 2010 , vol. 48, # 18 p. 4128 - 4139
反应条件
1.1: water; potassium hydroxide / ethanol / 6 h / Reflux 1.2: pH 2 2.1: 2,6-di-tert-butyl-4-methyl-phenol; triethylamine / tetrahydrofuran / 0 - 45 °C View Scheme
参考文献
Martinelli, Elisa; Paoli, Francesca; Gallot, Bernard; Galli, Giancarlo
Journal of Polymer Science, Part A: Polymer Chemistry, 2010 , vol. 48, # 18 p. 4128 - 4139
